2-Methyl-propane-2-sulfinic acid [(S)-2-dibenzylamino-4-methyl-pent-(E)-ylidene]-amide

Base Information

• Chemical Name: 2-Methyl-propane-2-sulfinic acid [(S)-2-dibenzylamino-4-methyl-pent-(E)-ylidene]-amide
• CAS No.: 441045-64-3
• Molecular Formula: C₂₄H₃₄N₂OS
• Molecular Weight: 398.613

Synonyms:2-Methyl-propane-2-sulfinic acid [(S)-2-dibenzylamino-4-methyl-pent-(E)-ylidene]-amide

Chemical Property of 2-Methyl-propane-2-sulfinic acid [(S)-2-dibenzylamino-4-methyl-pent-(E)-ylidene]-amide

Chemical Property:

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Technology Process of 2-Methyl-propane-2-sulfinic acid [(S)-2-dibenzylamino-4-methyl-pent-(E)-ylidene]-amide

There total 1 articles about 2-Methyl-propane-2-sulfinic acid [(S)-2-dibenzylamino-4-methyl-pent-(E)-ylidene]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(S)-2-(dibenzylamino)-4-methylpentanal (111060-65-2) + (R)-2-methylpropane-2-sulfinamide (196929-78-9) → 2-Methyl-propane-2-sulfinic acid [(S)-2-dibenzylamino-4-methyl-pent-(E)-ylidene]-amide (441045-64-3)

Guidance literature:

With titanium(IV) tetraethanolate; In tetrahydrofuran; at 0 - 20 ℃; for 6h;

DOI:10.1021/ja020482+

Reference yield: 83.0%

difluoromethyl phenyl sulfone (1535-65-5) + 2-Methyl-propane-2-sulfinic acid [(S)-2-dibenzylamino-4-methyl-pent-(E)-ylidene]-amide (441045-64-3) → C31H40F2N2O3S2

Guidance literature:

With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃;

DOI:10.1021/jo070094w

Reference yield: 71.0%

(trifluoromethyl)trimethylsilane (81290-20-2) + 2-Methyl-propane-2-sulfinic acid [(S)-2-dibenzylamino-4-methyl-pent-(E)-ylidene]-amide (441045-64-3) → (R)-N-((2S,3S)-3-(dibenzylamino)-1,1,1-trifluoro-5-methylhexan-2-yl)-2-methylpropane-2-sulfinamide

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -35 ℃; for 2h;

DOI:10.1021/ja020482+

upstream raw materials:

(S)-2-(dibenzylamino)-4-methylpentanal

(R)-2-methylpropane-2-sulfinamide

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