isopropyl 1-(l-p-menth-3-yloxy)-2-naphthoate

Base Information

Chemical Name:isopropyl 1-(l-p-menth-3-yloxy)-2-naphthoate
CAS No.:129656-74-2
Molecular Formula:C₂₄H₃₂O₃
Molecular Weight:368.516
Hs Code.:

Synonyms:isopropyl 1-(l-p-menth-3-yloxy)-2-naphthoate

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Chemical Property of isopropyl 1-(l-p-menth-3-yloxy)-2-naphthoate

Chemical Property:

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Technology Process of isopropyl 1-(l-p-menth-3-yloxy)-2-naphthoate

There total 7 articles about isopropyl 1-(l-p-menth-3-yloxy)-2-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1-(l-p-menth-3-yloxy)-2-naphthoyl chloride

: 67-63-0,8013-70-5
isopropyl alcohol

: 129656-74-2
isopropyl 1-(l-p-menth-3-yloxy)-2-naphthoate

Guidance literature:: With pyridine; dmap; In benzene; for 3h; Heating;
DOI:10.1246/bcsj.66.613

Reference yield:

: 6039-59-4
methyl 1-methoxy-2-naphthoate

: 129656-74-2
isopropyl 1-(l-p-menth-3-yloxy)-2-naphthoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) from 65 deg C to 90 deg C, 2.) DMF, 50 deg C, 1 h

2: 79 percent / aq.-ethanolic KOH / 10 h / Heating

3: SOCl₂ / 3 h / Heating

4: 79 percent / 4-dimethylaminopyridine (DMAP), pyridine / benzene / 3 h / Heating

With pyridine; dmap; potassium hydroxide; thionyl chloride; sodium hydride; In benzene;
DOI:10.1246/bcsj.66.613

Reference yield:

: 129656-73-1
(-)-menthyl 1-(-)-menthyloxy-2-naphthoate

: 129656-74-2
isopropyl 1-(l-p-menth-3-yloxy)-2-naphthoate

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / aq.-ethanolic KOH / 10 h / Heating

2: SOCl₂ / 3 h / Heating

3: 79 percent / 4-dimethylaminopyridine (DMAP), pyridine / benzene / 3 h / Heating

With pyridine; dmap; potassium hydroxide; thionyl chloride; In benzene;
DOI:10.1246/bcsj.66.613