N-SES-D-Ser-Pip-OBn

Base Information

Chemical Name:N-SES-D-Ser-Pip-OBn
CAS No.:151961-22-7
Molecular Formula:C₃₇H₆₁N₅O₁₁SSi
Molecular Weight:812.07
Hs Code.:

N-SES-D-Ser<Boc-Gly-Sar-NMe-Val>-Pip-OBn

Synonyms:N-SES-D-Ser-Pip-OBn

Suppliers and Price of N-SES-D-Ser-Pip-OBn

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-SES-D-Ser-Pip-OBn

Chemical Property:

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Technology Process of N-SES-D-Ser-Pip-OBn

There total 21 articles about N-SES-D-Ser-Pip-OBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 151961-21-6
Boc-Gly-Sar-NMe-Val-OH

: 174311-11-6
N-SES-D-Ser-Pip-OBn

: 151961-22-7
N-SES-D-Ser-Pip-OBn

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 24h;
DOI:10.1021/ja00077a082

Reference yield: 50.0%

: 151961-21-6
Boc-Gly-Sar-NMe-Val-OH

: 174311-11-6
N-SES-D-Ser-Pip-OBn

: 151961-22-7
N-SES-D-Ser-Pip-OBn

: (S)-1-[(R)-3-[(R)-2-({2-[(2-tert-Butoxycarbonylamino-acetyl)-methyl-amino]-acetyl}-methyl-amino)-3-methyl-butyryloxy]-2-(2-trimethylsilanyl-ethanesulfonylamino)-propionyl]-piperidine-2-carboxylic acid benzyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 24h;
DOI:10.1021/ja952799y

Reference yield:

: 133498-97-2
t-BuOCO-Gly-Sar-OH

: 151961-22-7
N-SES-D-Ser-Pip-OBn

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / Et₃N, DCC, DMAP / CH₂Cl₂ / 24 h / 25 °C

2: 90 percent / LiOH*H₂O / tetrahydrofuran; methanol; H₂O / 3 h / 25 °C

3: 50 percent / DMAP, DCC / CH₂Cl₂ / 24 h / 0 °C

With dmap; lithium hydroxide; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja952799y