ethyl 2-(4-(4-(2-carbamoyl-2-(4-methylbenzyl)hydrazinyl)-4-oxobutyl)phenoxy)-2-methylpropanoate

Base Information

Chemical Name:ethyl 2-(4-(4-(2-carbamoyl-2-(4-methylbenzyl)hydrazinyl)-4-oxobutyl)phenoxy)-2-methylpropanoate
CAS No.:1128073-03-9
Molecular Formula:C₂₅H₃₃N₃O₅
Molecular Weight:455.554
Hs Code.:

Synonyms:ethyl 2-(4-(4-(2-carbamoyl-2-(4-methylbenzyl)hydrazinyl)-4-oxobutyl)phenoxy)-2-methylpropanoate

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Chemical Property of ethyl 2-(4-(4-(2-carbamoyl-2-(4-methylbenzyl)hydrazinyl)-4-oxobutyl)phenoxy)-2-methylpropanoate

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Technology Process of ethyl 2-(4-(4-(2-carbamoyl-2-(4-methylbenzyl)hydrazinyl)-4-oxobutyl)phenoxy)-2-methylpropanoate

There total 8 articles about ethyl 2-(4-(4-(2-carbamoyl-2-(4-methylbenzyl)hydrazinyl)-4-oxobutyl)phenoxy)-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-[(4-methylphenyl)methyl]hydrazinecarboxamide monomethanesulfonate

: 4-[4-(1-ethoxycarbonyl-1-methylethoxy)phenyl]butyric acid chloride

: 1128073-03-9
ethyl 2-(4-(4-(2-carbamoyl-2-(4-methylbenzyl)hydrazinyl)-4-oxobutyl)phenoxy)-2-methylpropanoate

Guidance literature:: With pyridine; In ethyl acetate; at 20 ℃; for 1h; Large scale;
DOI:10.1021/op700040v

Reference yield:

: 4-[4-(1-ethoxycarbonyl-1-methylethoxy)phenyl]butyric acid chloride

: 425675-44-1
1-[(4-methylphenyl)methyl]hydrazinecarboxamide

: 1128073-03-9
ethyl 2-(4-(4-(2-carbamoyl-2-(4-methylbenzyl)hydrazinyl)-4-oxobutyl)phenoxy)-2-methylpropanoate

Guidance literature:: With pyridine; In toluene; at 25 ℃; for 1h; Inert atmosphere; Large scale reaction;
DOI:10.1021/op8002486

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 1128073-03-9
ethyl 2-(4-(4-(2-carbamoyl-2-(4-methylbenzyl)hydrazinyl)-4-oxobutyl)phenoxy)-2-methylpropanoate

Guidance literature:: Multi-step reaction with 5 steps

1: hydrazine

2: hydrogen; palladium 10% on activated carbon / ethanol / 20 °C / 3345.86 Torr

3: isopropyl alcohol / 16 h / 20 °C

4: isopropyl alcohol

5: pyridine / ethyl acetate / 1 h / 20 °C / Large scale

With pyridine; palladium 10% on activated carbon; hydrogen; hydrazine; In ethanol; ethyl acetate; isopropyl alcohol;
DOI:10.1021/op700040v