2-(4-Keto-cyclohexen-⁽¹⁾-yl)-ethylalkohol

Base Information

• Chemical Name: 2-(4-Keto-cyclohexen-⁽¹⁾-yl)-ethylalkohol
• CAS No.: 90199-14-7
• Molecular Formula: C₈H₁₂O₂
• Molecular Weight: 140.182
• Mol file: 90199-14-7.mol

Synonyms:2-(4-Keto-cyclohexen-⁽¹⁾-yl)-ethylalkohol

Chemical Property of 2-(4-Keto-cyclohexen-⁽¹⁾-yl)-ethylalkohol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-Keto-cyclohexen-⁽¹⁾-yl)-ethylalkohol

There total 2 articles about 2-(4-Keto-cyclohexen-⁽¹⁾-yl)-ethylalkohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-Methoxyphenyl)ethanol (702-23-8) → 2-(4-Keto-cyclohexen-(1)-yl)-ethylalkohol (90199-14-7)

Guidance literature:

With ammonia; oxalic acid; lithium; tert-butyl alcohol; Multistep reaction;

DOI:10.1021/ja00037a061

Reference yield:

→ 2-(4-Keto-cyclohexen-(1)-yl)-ethylalkohol (90199-14-7)

Guidance literature:

2-(2,5-Dihydro-4-methoxy-phenyl)-ethylalkohol IIa, H2SO4, Tetrahydrofuran, W.;

DOI:10.1021/jo01052a507

Reference yield:

2-(4-Keto-cyclohexen-(1)-yl)-ethylalkohol (90199-14-7) + tert-butyldimethylsilyl chloride (18162-48-6) → C14H26O2Si

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

DOI:10.1016/j.tetlet.2016.08.096

upstream raw materials:

2-(4-Methoxyphenyl)ethanol

Downstream raw materials:

(4-oxocyclohexyl)acetaldehyde

4-<(2Z)-3-(methoxycarbonyl)-2-propenyl>cyclohexan-1-one

4-<(2E)-3-(methoxycarbonyl)-2-propenyl>cyclohexan-1-one

(R)-2-(4-oxocyclohex-2-en-1-yl)ethyl 4-chlorobenzoate