methanesulfonic acid 6-[3,5-bis-(6-methanesulfonyloxy-hexyloxymethyl)-2,4,6-trimethyl-benzyloxy]-hexyl ester

Base Information

Chemical Name:methanesulfonic acid 6-[3,5-bis-(6-methanesulfonyloxy-hexyloxymethyl)-2,4,6-trimethyl-benzyloxy]-hexyl ester
CAS No.:911854-35-8
Molecular Formula:C₃₃H₆₀O₁₂S₃
Molecular Weight:745.03
Hs Code.:

Synonyms:methanesulfonic acid 6-[3,5-bis-(6-methanesulfonyloxy-hexyloxymethyl)-2,4,6-trimethyl-benzyloxy]-hexyl ester

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Chemical Property of methanesulfonic acid 6-[3,5-bis-(6-methanesulfonyloxy-hexyloxymethyl)-2,4,6-trimethyl-benzyloxy]-hexyl ester

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Technology Process of methanesulfonic acid 6-[3,5-bis-(6-methanesulfonyloxy-hexyloxymethyl)-2,4,6-trimethyl-benzyloxy]-hexyl ester

There total 4 articles about methanesulfonic acid 6-[3,5-bis-(6-methanesulfonyloxy-hexyloxymethyl)-2,4,6-trimethyl-benzyloxy]-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 911854-34-7
6,6',6''-(((2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene))tris(oxy))tris(hexan-1-ol)

: 124-63-0
methanesulfonyl chloride

: 911854-35-8
methanesulfonic acid 6-[3,5-bis-(6-methanesulfonyloxy-hexyloxymethyl)-2,4,6-trimethyl-benzyloxy]-hexyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 25 ℃; for 10h;
DOI:10.1021/ol0615026

Reference yield:

: 911854-39-2
C₄₅H₇₈O₉

: 911854-35-8
methanesulfonic acid 6-[3,5-bis-(6-methanesulfonyloxy-hexyloxymethyl)-2,4,6-trimethyl-benzyloxy]-hexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 3.3 g / p-TsOH / methanol / 12 h / 25 °C

2: 79 percent / triethylamine / CH₂Cl₂ / 10 h / 0 - 25 °C

With toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane;
DOI:10.1021/ol0615026

Reference yield:

: 28659-22-5
6-(tetrahydro-2H-pyranyloxy)hexan-1-ol

: 911854-35-8
methanesulfonic acid 6-[3,5-bis-(6-methanesulfonyloxy-hexyloxymethyl)-2,4,6-trimethyl-benzyloxy]-hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / tetrahydrofuran / 18 h / 80 °C

2: 3.3 g / p-TsOH / methanol / 12 h / 25 °C

3: 79 percent / triethylamine / CH₂Cl₂ / 10 h / 0 - 25 °C

With sodium hydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol0615026