2-Phenyl-Δ^1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone

Base Information

• Chemical Name: 2-Phenyl-Δ^1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone
• CAS No.: 74879-74-6
• Molecular Formula: C₂₅H₃₀N₄
• Molecular Weight: 386.54

Synonyms:2-Phenyl-Δ^1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone

Chemical Property of 2-Phenyl-Δ^1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Phenyl-Δ^1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone

There total 3 articles about 2-Phenyl-Δ^1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

2,2'-methylenedicyclohexanone diphenylhydrazone (87268-51-7) → 2-Phenyl-Δ1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone (74879-74-6)

Guidance literature:

With oxygen; In benzene;

DOI:10.1007/BF00523082

Reference yield:

phenylhydrazine (100-63-0) → 2-Phenyl-Δ1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone (74879-74-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / ethanol / 10 h

2: 53 percent / O₂ / benzene

With oxygen; In ethanol; benzene;

DOI:10.1007/BF00523082

Reference yield:

bis(2-oxocyclohexyl)methane (3137-39-1) → 2-Phenyl-Δ1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone (74879-74-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / ethanol / 10 h

2: 53 percent / O₂ / benzene

With oxygen; In ethanol; benzene;

DOI:10.1007/BF00523082

upstream raw materials:

2,2'-methylenedicyclohexanone diphenylhydrazone

phenylhydrazine

bis(2-oxocyclohexyl)methane

Downstream raw materials:

2-Phenyl-Δ^1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one

1,2,3,4-Tetrahydrocarbazole-1-spiro-3'-(2'-phenyl-Δ^1'(8'a)-octahydrocinnoline)

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 74879-74-6 2-Phenyl-Δ^1(8a)-octahydrocinnoline-3-spiro-1'-cyclohexan-2'-one Phenylhydrazone

Send

Send

Metric Ton KG G Pound L ML

Send

Send