C₁₄H₁₄F₂O₄

Base Information

Chemical Name:C₁₄H₁₄F₂O₄
CAS No.:1443154-40-2
Molecular Formula:C₁₄H₁₄F₂O₄
Molecular Weight:284.26
Hs Code.:

C<sub>14</sub>H<sub>14</sub>F<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₄H₁₄F₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₄F₂O₄

Chemical Property:

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Technology Process of C₁₄H₁₄F₂O₄

There total 1 articles about C₁₄H₁₄F₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 437-81-0
2,6-difluorobenzaldehyde

: 105-53-3
diethyl malonate

: 1443154-40-2
C₁₄H₁₄F₂O₄

Guidance literature:: With piperidine; In 5,5-dimethyl-1,3-cyclohexadiene; Reflux; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201203891

Reference yield: 90.0%

: 1443154-40-2
C₁₄H₁₄F₂O₄

: 555-21-5,34512-13-5,174848-08-9
4-Nitrophenylacetonitrile

: diethyl 2-((1R,2R)-2-cyano-1-(2,6-difluorophenyl)-2-(4-nitrophenyl)ethyl)malonate

Guidance literature:: 4-Nitrophenylacetonitrile; With C₄₃H₆₄N₄O₄; bis((1,1,1-trifluoro-N-(trifluoromethyl)sulfonyl)methylsulfonamido)zinc; In 1,2-dichloro-ethane; at 35 ℃; for 0.5h; Sealed tube;

C₁₄H₁₄F₂O₄; In 1,2-dichloro-ethane; at 15 ℃; for 44h; enantioselective reaction; Sealed tube;
DOI:10.1002/chem.201302122

Reference yield:

: 1443154-40-2
C₁₄H₁₄F₂O₄

: 17822-51-4
1-benzylidene-3-oxo-1-pyrazolidinium-2-ide

: (1R,3S)-diethyl 3-(2,6-difluorophenyl)-5-oxo-1-phenyltetrahydropyrazolo[1,2-a]pyrazole-2,2(1H)-dicarboxylate

: (1S,3R)-diethyl 3-(2,6-difluorophenyl)-5-oxo-1-phenyltetrahydropyrazolo[1,2-a]pyrazole-2,2(1H)-dicarboxylate

Guidance literature:: With C₂₃H₄₄N₄O₄; nickel(II) perchlorate hexahydrate; In dichloromethane; at 30 ℃; for 28h; Overall yield = 90 %; enantioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201203891