bis-(2-bromomethyl-phenyl)-sulfane

Base Information

Chemical Name:bis-(2-bromomethyl-phenyl)-sulfane
CAS No.:32636-05-8
Molecular Formula:C₁₄H₁₂Br₂S
Molecular Weight:372.123
Hs Code.:

Synonyms:bis-(2-bromomethyl-phenyl)-sulfane

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Chemical Property of bis-(2-bromomethyl-phenyl)-sulfane

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Technology Process of bis-(2-bromomethyl-phenyl)-sulfane

There total 10 articles about bis-(2-bromomethyl-phenyl)-sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 4537-05-7
du-o-tolyl sulfide

: 32636-05-8
bis-(2-bromomethyl-phenyl)-sulfane

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 12h; Product distribution / selectivity; Heating / reflux;

Reference yield:

: 88-65-3
2-bromobenzoic-acid

: 32636-05-8
bis-(2-bromomethyl-phenyl)-sulfane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / copper / water / 3 h / 130 - 140 °C

2: borane-THF / tetrahydrofuran / 16 h / 20 °C

3: phosphorus tribromide / diethyl ether / 3 h / 20 °C

With borane-THF; phosphorus tribromide; potassium carbonate; copper; In tetrahydrofuran; diethyl ether; water; 1: Ullmann Condensation;

Reference yield:

: 147-93-3
Thiosalicylic acid

: 32636-05-8
bis-(2-bromomethyl-phenyl)-sulfane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / copper / water / 3 h / 130 - 140 °C

2: borane-THF / tetrahydrofuran / 16 h / 20 °C

3: phosphorus tribromide / diethyl ether / 3 h / 20 °C

With borane-THF; phosphorus tribromide; potassium carbonate; copper; In tetrahydrofuran; diethyl ether; water; 1: Ullmann Condensation;