1-methyl-3-[(S)-3-N-(tert-butoxycarbonyl)amino-3-methoxycarbonylpropyl]-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine

Base Information

Chemical Name:1-methyl-3-[(S)-3-N-(tert-butoxycarbonyl)amino-3-methoxycarbonylpropyl]-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine
CAS No.:1024616-77-0
Molecular Formula:C₃₉H₅₃N₃O₁₀Si
Molecular Weight:751.949
Hs Code.:

Synonyms:1-methyl-3-[(S)-3-N-(tert-butoxycarbonyl)amino-3-methoxycarbonylpropyl]-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-methyl-3-[(S)-3-N-(tert-butoxycarbonyl)amino-3-methoxycarbonylpropyl]-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine

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Technology Process of 1-methyl-3-[(S)-3-N-(tert-butoxycarbonyl)amino-3-methoxycarbonylpropyl]-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine

There total 1 articles about 1-methyl-3-[(S)-3-N-(tert-butoxycarbonyl)amino-3-methoxycarbonylpropyl]-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1024616-73-6
1-methyl-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine

: 120042-11-7,258351-86-9
methyl (S)-4-hydroxy-2-((tert-butoxy)carbonylamino)-butyrate

: 1024616-77-0
1-methyl-3-[(S)-3-N-(tert-butoxycarbonyl)amino-3-methoxycarbonylpropyl]-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2007.11.039

Reference yield: 92.0%

: 1024616-77-0
1-methyl-3-[(S)-3-N-(tert-butoxycarbonyl)amino-3-methoxycarbonylpropyl]-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine

: 1024616-79-2,52777-29-4
1-methyl-3-(3-amino-3-carboxypropyl)pseudouridine

Guidance literature:: 1-methyl-3-[(S)-3-N-(tert-butoxycarbonyl)amino-3-methoxycarbonylpropyl]-5'-O-(tert-butyldiphenylsilyl)-2',3'-O-(isopropylidene)pseudouridine; With sodium hydroxide; In 1,4-dioxane; at 20 ℃; for 0.5h;

With trifluoroacetic acid; at 20 ℃; for 1h; Further stages.;
DOI:10.1016/j.bmc.2007.11.039