4-(2-(4-morpholinophenylamino)-5-methylpyrimidin-4-yl)-2-methoxybenzoic acid sodium salt

Base Information

Chemical Name:4-(2-(4-morpholinophenylamino)-5-methylpyrimidin-4-yl)-2-methoxybenzoic acid sodium salt
CAS No.:1056635-40-5
Molecular Formula:C₂₃H₂₃N₄O₄*Na
Molecular Weight:442.45
Hs Code.:

Synonyms:4-(2-(4-morpholinophenylamino)-5-methylpyrimidin-4-yl)-2-methoxybenzoic acid sodium salt

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Chemical Property of 4-(2-(4-morpholinophenylamino)-5-methylpyrimidin-4-yl)-2-methoxybenzoic acid sodium salt

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Technology Process of 4-(2-(4-morpholinophenylamino)-5-methylpyrimidin-4-yl)-2-methoxybenzoic acid sodium salt

There total 3 articles about 4-(2-(4-morpholinophenylamino)-5-methylpyrimidin-4-yl)-2-methoxybenzoic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1056634-62-8
ethyl 4-(2-(4-morpholinophenylamino)pyrimidin-4-yl)benzoate

: 1056635-40-5
4-(2-(4-morpholinophenylamino)-5-methylpyrimidin-4-yl)-2-methoxybenzoic acid sodium salt

Guidance literature:: With methanol; sodium hydroxide; water; In tetrahydrofuran; Heating / reflux;

Reference yield:

: 4334-88-7
p-ethoxycarbonylphenylboronic acid

: 1056635-40-5
4-(2-(4-morpholinophenylamino)-5-methylpyrimidin-4-yl)-2-methoxybenzoic acid sodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 75 - 100 °C

2: toluene-4-sulfonic acid / 1,4-dioxane / Heating / reflux

3: methanol; sodium hydroxide; water / tetrahydrofuran / Heating / reflux

With methanol; sodium hydroxide; water; sodium carbonate; toluene-4-sulfonic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; toluene; 1: Suzuki Coupling;

Reference yield:

: 499195-60-7
4-(4-carboethoxyphenyl)-2-chloropyrimidine

: 1056635-40-5
4-(2-(4-morpholinophenylamino)-5-methylpyrimidin-4-yl)-2-methoxybenzoic acid sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / 1,4-dioxane / Heating / reflux

2: methanol; sodium hydroxide; water / tetrahydrofuran / Heating / reflux

With methanol; sodium hydroxide; water; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane;