cis-1-amino-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Base Information

• Chemical Name: cis-1-amino-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide
• CAS No.: 158786-83-5
• Molecular Formula: C₁₆H₂₂N₂O₃S
• Molecular Weight: 322.428

Synonyms:cis-1-amino-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Chemical Property of cis-1-amino-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Chemical Property:

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Technology Process of cis-1-amino-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

There total 7 articles about cis-1-amino-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N,N-Pentamethylene-cis-3-(phenylsulfonyl)-1-triazenocyclobutane-1-carboxamide (158786-79-9) → cis-1-amino-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide (158786-83-5)

Guidance literature:

Heating;

DOI:10.1021/jm00051a005

Reference yield:

cis-1-Azido-N,N-pentamethylene-3-(phenylsulfonyl)cyclobutane-1-carboxamide (117488-02-5) → N,N-Pentamethylene-cis-3-(phenylsulfonyl)-1-triazenocyclobutane-1-carboxamide (158786-79-9) + cis-1-amino-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide (158786-83-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 20h; under 760 Torr;

DOI:10.1021/jm00051a005

Reference yield:

cis-1-Azido-N,N-pentamethylene-3-(phenylsulfonyl)cyclobutane-1-carboxamide (117488-02-5) → cis-1-amino-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide (158786-83-5)

Guidance literature:

With palladium on activated charcoal; ammonium formate; In methanol; at 50 ℃; for 5h;

upstream raw materials:

cis-1-Azido-N,N-pentamethylene-3-(phenylsulfonyl)cyclobutane-1-carboxamide

N,N-Pentamethylene-cis-3-(phenylsulfonyl)-1-triazenocyclobutane-1-carboxamide

(3-Benzenesulfonyl-bicyclo[1.1.0]but-1-yl)-piperidin-1-yl-methanone

3-Benzenesulfonyl-bicyclo[1.1.0]butane-1-carboxylic acid

Downstream raw materials:

trans-1-(benzoylamino)-3-<2-(dimethoxyphosphoryl)acetyl>cyclobutane-1-N,N-pentamethylenecarboxamide

cis-1-(benzoylamino)-3-<2-(dimethoxyphosphoryl)acetyl>cyclobutane-1-N,N-pentamethylenecarboxamide

trans-1-(benzoylamino)-3-<2-(dimethoxyphosphoryl)ethyl>cyclobutane-1-N,N-pentamethylenecarboxamide

cis-1-(benzoylamino)-3-<2-(dimethoxyphosphoryl)-ethyl>cyclobutane-1-N,N-pentamethylenecarboxamide

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