cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Base Information

Chemical Name:cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide
CAS No.:158786-87-9
Molecular Formula:C₂₃H₂₆N₂O₄S
Molecular Weight:426.536
Hs Code.:

Synonyms:cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Suppliers and Price of cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

There total 8 articles about cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117488-02-5
cis-1-Azido-N,N-pentamethylene-3-(phenylsulfonyl)cyclobutane-1-carboxamide

: 158786-87-9
cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium formate, 10percent Pd/C / methanol / 5 h / 50 °C

2: pyridine / CH₂Cl₂

With pyridine; palladium on activated charcoal; ammonium formate; In methanol; dichloromethane;

Reference yield:

: 124291-40-3
3-Benzenesulfonyl-bicyclo[1.1.0]butane-1-carboxylic acid

: 158786-87-9
cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / TMG, NaN₃ / dimethylformamide / 6 h / 90 °C

2: SOCl₂ / 1 h / 75 °C

3: CH₂Cl₂ / 1 h / Ambient temperature

4: H₂ / Pd/C / ethyl acetate / 20 h / 760 Torr

5: 96 percent / Heating

6: Et₃N / 1 h / 0 - 20 °C

With thionyl chloride; sodium azide; hydrogen; triethylamine; N,N,N',N'-tetramethylguanidine; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00051a005

Reference yield:

: 161181-43-7
1-Azido-3-benzenesulfonyl-cyclobutanecarbonyl chloride

: 158786-87-9
cis-1-(benzoylamino)-3-(phenylsulfonyl)cyclobutane-1-N,N-pentamethylenecarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 1 h / Ambient temperature

2: H₂ / Pd/C / ethyl acetate / 20 h / 760 Torr

3: 96 percent / Heating

4: Et₃N / 1 h / 0 - 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm00051a005