tert-butyldiphenylsilyl 3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:tert-butyldiphenylsilyl 3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:1219595-38-6
Molecular Formula:C₄₅H₅₅N₃O₁₀Si
Molecular Weight:826.031
Hs Code.:

Synonyms:tert-butyldiphenylsilyl 3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyldiphenylsilyl 3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of tert-butyldiphenylsilyl 3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 1 articles about tert-butyldiphenylsilyl 3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 67-64-1
acetone

: (2S,3R,4S,5R,6R)-2-[(2R,3S,4R,5R,6S)-5-Azido-4-benzyloxy-2-benzyloxymethyl-6-(tert-butyl-diphenyl-silanyloxy)-tetrahydro-pyran-3-yloxy]-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

: 1219595-38-6
tert-butyldiphenylsilyl 3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1219595-39-7
C₄₅H₅₅N₃O₁₀Si

Guidance literature:: With toluene-4-sulfonic acid; copper(II) sulfate; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2009.12.031

Reference yield: 86.0%

: 1219595-38-6
tert-butyldiphenylsilyl 3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 100-39-0
benzyl bromide

: 213591-34-5
tert-butyldiphenylsilyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: tert-butyldiphenylsilyl 3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside; With sodium hydride; In tetrahydrofuran; mineral oil; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; mineral oil; at 60 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2009.12.031