C₂₇H₃₁NO₁₀

Base Information

Chemical Name:C₂₇H₃₁NO₁₀
CAS No.:1313375-90-4
Molecular Formula:C₂₇H₃₁NO₁₀
Molecular Weight:529.544
Hs Code.:

C<sub>27</sub>H<sub>31</sub>NO<sub>10</sub>

Synonyms:C₂₇H₃₁NO₁₀

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Chemical Property of C₂₇H₃₁NO₁₀

Chemical Property:

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Technology Process of C₂₇H₃₁NO₁₀

There total 6 articles about C₂₇H₃₁NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1313375-27-7
C₁₆H₂₀O₇

: 108-24-7
acetic anhydride

: 2450-71-7
Propargylamine

: 1313375-90-4
C₂₇H₃₁NO₁₀

Guidance literature:: C₁₆H₂₀O₇; Propargylamine; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;

acetic anhydride; With pyridine; dmap; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1002/chem.201003402

Reference yield:

: 1071472-86-0
methyl (E)-4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-but-2-enoate

: 1313375-90-4
C₂₇H₃₁NO₁₀

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere

2.1: sodium methylate / methanol / 24 h / 20 °C

3.1: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

4.2: 20 °C

With tetrabutylammomium bromide; water; sodium methylate; palladium diacetate; sodium hydrogencarbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; 1.1: Heck coupling / 2.1: Zemplen reaction;
DOI:10.1002/chem.201003402

Reference yield:

: 1071472-93-9
(E)-methyl 2-phenyl-4-(β-D-galactopyranosyl)but-2-enoate

: 1313375-90-4
C₂₇H₃₁NO₁₀

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

2.2: 20 °C

With water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201003402