methyl 3-[3-ethyl-5-(6-phenylpyridin-3-yl)-4H-1,2,4-triazol-4-yl]-2-methylbenzoate

Base Information

Chemical Name:methyl 3-[3-ethyl-5-(6-phenylpyridin-3-yl)-4H-1,2,4-triazol-4-yl]-2-methylbenzoate
CAS No.:1416057-64-1
Molecular Formula:C₂₄H₂₂N₄O₂
Molecular Weight:398.464
Hs Code.:

Synonyms:methyl 3-[3-ethyl-5-(6-phenylpyridin-3-yl)-4H-1,2,4-triazol-4-yl]-2-methylbenzoate

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Chemical Property of methyl 3-[3-ethyl-5-(6-phenylpyridin-3-yl)-4H-1,2,4-triazol-4-yl]-2-methylbenzoate

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Technology Process of methyl 3-[3-ethyl-5-(6-phenylpyridin-3-yl)-4H-1,2,4-triazol-4-yl]-2-methylbenzoate

There total 5 articles about methyl 3-[3-ethyl-5-(6-phenylpyridin-3-yl)-4H-1,2,4-triazol-4-yl]-2-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1416057-63-0
methyl 3-{[hydrazino(6-phenylpyridin-3-yl)methylene]amino}-2-methylbenzoate

: 78-39-7
Triethyl orthoacetate

: 1416057-64-1
methyl 3-[3-ethyl-5-(6-phenylpyridin-3-yl)-4H-1,2,4-triazol-4-yl]-2-methylbenzoate

Guidance literature:: In ethanol; for 1h; Reflux;
DOI:10.1016/j.tetasy.2012.10.005

Reference yield:

: C₂₁H₁₉ClN₂O₂

: 1416057-64-1
methyl 3-[3-ethyl-5-(6-phenylpyridin-3-yl)-4H-1,2,4-triazol-4-yl]-2-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 1 h / 20 °C

2: ethanol / 1 h / Reflux

With hydrazine hydrate; In ethanol;
DOI:10.1016/j.tetasy.2012.10.005

Reference yield:

: 29051-44-3
6-phenylpyridine-3-carboxylic acid

: 1416057-64-1
methyl 3-[3-ethyl-5-(6-phenylpyridin-3-yl)-4H-1,2,4-triazol-4-yl]-2-methylbenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 1 h / 60 °C

2: pyridine / tetrahydrofuran / 1 h / 0 - 20 °C

3: thionyl chloride / 1 h / 80 °C

4: hydrazine hydrate / ethanol / 1 h / 20 °C

5: ethanol / 1 h / Reflux

With pyridine; thionyl chloride; hydrazine hydrate; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tetasy.2012.10.005