C₅₃H₈₀O₆Si₃IN

Base Information

Chemical Name:C₅₃H₈₀O₆Si₃IN
CAS No.:936824-93-0
Molecular Formula:C₅₃H₈₀INO₆Si₃
Molecular Weight:1038.38
Hs Code.:

C<sub>53</sub>H<sub>80</sub>O<sub>6</sub>Si<sub>3</sub>IN

Synonyms:C₅₃H₈₀O₆Si₃IN

Suppliers and Price of C₅₃H₈₀O₆Si₃IN

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₃H₈₀O₆Si₃IN

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₃H₈₀O₆Si₃IN

There total 4 articles about C₅₃H₈₀O₆Si₃IN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: C₂₇H₅₂O₆Si₂

: 936824-91-8
3-(tert-butyl-diphenyl-silanyloxy)-5-[(E)-3-iodo-2-methylallyl]-phenylamine

: 936824-93-0
C₅₃H₈₀O₆Si₃IN

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/ol0702270

Reference yield:

: 875439-73-9
3-amino-5-[(E)-3-iodo-2-methylprop-2-enyl]-phenol

: 936824-93-0
C₅₃H₈₀O₆Si₃IN

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / imidazole; DMAP / CH₂Cl₂ / 1.5 h

2: 70 percent / N,N-bis(2-oxo-3-oxazolidinyl)phosphonic acid chloride; DIEA / CH₂Cl₂ / 18 h / 20 °C

With 1H-imidazole; dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ol0702270

Reference yield:

: 875439-71-7
3-[3-tert-butoxycarbonylamino-5-(tert-butyl-diphenyl-silanyloxy)-phenyl]-1-trimethylsilyl-propyne

: 936824-93-0
C₅₃H₈₀O₆Si₃IN

Guidance literature:: Multi-step reaction with 4 steps

1.1: 88 percent / tetra-n-butylammonium fluoride trihydrate / tetrahydrofuran / -20 - 0 °C

2.1: Cp₂ZrCl₂ / hexane; 1,2-dichloro-ethane / 0.83 h / 0 - 20 °C

2.2: 1,2-dichloro-ethane; hexane / 72 h / 20 °C

2.3: 58 percent / iodine / 1,2-dichloro-ethane; hexane; tetrahydrofuran / -30 - 0 °C

3.1: 94 percent / imidazole; DMAP / CH₂Cl₂ / 1.5 h

4.1: 70 percent / N,N-bis(2-oxo-3-oxazolidinyl)phosphonic acid chloride; DIEA / CH₂Cl₂ / 18 h / 20 °C

With 1H-imidazole; dmap; zirconocene dichloride; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol0702270