tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethyl radical

Base Information

• Chemical Name: tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethyl radical
• CAS No.: 101981-08-2
• Molecular Formula: C₂₇H₁₃Cl₁₄O₄
• Molecular Weight: 897.74

Synonyms:tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethyl radical

Chemical Property of tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethyl radical

Chemical Property:

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Technology Process of tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethyl radical

There total 2 articles about tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

4-(bromomethyl)tetradecachlorotriphenylmethyl radical (81221-80-9) + diethyl malonate (105-53-3) → tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethyl radical (101981-08-2)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; for 1.16667h; Heating;

DOI:10.1021/jo00363a013

Reference yield:

4-(bromomethyl)tetradecachlorotriphenylmethyl radical (81221-80-9) + 6,6'-((4-(bromomethyl)-2,3,5,6-tetrachlorophenyl)methylene)bis(1,2,3,4,5-pentachlorobenzene) (101998-20-3) + diethyl malonate (105-53-3) → αH-tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethane (101980-96-5) + tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethyl radical (101981-08-2)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; at 90 ℃;

DOI:10.1039/c39830000982

Reference yield: 83.0%

tetradecachloro-4-(2,2-bis(ethoxycarbonyl)ethyl)triphenylmethyl radical (101981-08-2) → 4-(2-carboxyethyl)tetradecachlorotriphenylmethyl radical (101981-05-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 22h; Heating;

DOI:10.1021/jo00363a013

upstream raw materials:

4-(bromomethyl)tetradecachlorotriphenylmethyl radical

6,6'-((4-(bromomethyl)-2,3,5,6-tetrachlorophenyl)methylene)bis(1,2,3,4,5-pentachlorobenzene)

diethyl malonate

Downstream raw materials:

4-(2-carboxyethyl)tetradecachlorotriphenylmethyl radical

tetradecachloro-4-(2-(chlorocarbonyl)ethyl)triphenylmethyl radical

4-(2-(alaninocarbonyl)ethyl)tetradecachlorotriphenylmethyl radical ethyl ester

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