methyl 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

Base Information

Chemical Name:methyl 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate
CAS No.:1417418-29-1
Molecular Formula:C₂₃H₂₅BO₅
Molecular Weight:392.26
Hs Code.:

Synonyms:methyl 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

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Chemical Property of methyl 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

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Technology Process of methyl 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

There total 2 articles about methyl 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 22955-77-7
methyl 1-indanone-2-carboxylate

: 1417418-33-7
(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate

: 1417418-29-1
methyl 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

Guidance literature:: methyl 1-indanone-2-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate; With 1,1-Diphenylethylene; In N,N-dimethyl-formamide; for 4h; Inert atmosphere;
DOI:10.1002/anie.201206917

Reference yield:

: 99770-93-1
benzene-1,4-diboronic acid bispinacol ester

: 1417418-29-1
methyl 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / dichloromethane; 2,2,2-trifluoroethanol / 6 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2.2: 4 h / Inert atmosphere

With sodium hydride; acetic acid; In dichloromethane; 2,2,2-trifluoroethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201206917