(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate

Base Information

Chemical Name:(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate
CAS No.:1417418-33-7
Molecular Formula:C₂F₃O₂*C₁₉H₂₃BIO₃
Molecular Weight:550.121
Hs Code.:

Synonyms:(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate

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Chemical Property of (4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate

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Technology Process of (4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate

There total 1 articles about (4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 16308-14-8
4-methoxy(diacetoxyiodo)benzene

: 99770-93-1
benzene-1,4-diboronic acid bispinacol ester

: 76-05-1
trifluoroacetic acid

: 1417418-33-7
(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate

Guidance literature:: With acetic acid; In dichloromethane; 2,2,2-trifluoroethanol; at 20 ℃; for 6h; regioselective reaction;
DOI:10.1002/anie.201206917

Reference yield: 70.0%

: 1417418-33-7
(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate

: 135-19-3
β-naphthol

: 1417418-30-4
4,4,5,5-tetramethyl-2-(4-(naphthalen-2-yloxy)phenyl)-1,3,2-dioxaborolane

Guidance literature:: β-naphthol; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate; In tetrahydrofuran; at 40 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201206917

Reference yield: 55.0%

: 22955-77-7
methyl 1-indanone-2-carboxylate

: 1417418-33-7
(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate

: 1417418-29-1
methyl 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

Guidance literature:: methyl 1-indanone-2-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

(4-methoxyphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)iodonium trifluoroacetate; With 1,1-Diphenylethylene; In N,N-dimethyl-formamide; for 4h; Inert atmosphere;
DOI:10.1002/anie.201206917