2-(2-(2-(4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenoxy)ethoxy)ethoxy)ethanol

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Chemical Name:2-(2-(2-(4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenoxy)ethoxy)ethoxy)ethanol
CAS No.:946052-62-6
Molecular Formula:C₂₂H₂₈N₄O₄
Molecular Weight:412.489
Hs Code.:

Synonyms:2-(2-(2-(4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenoxy)ethoxy)ethoxy)ethanol

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Chemical Property of 2-(2-(2-(4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenoxy)ethoxy)ethoxy)ethanol

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Technology Process of 2-(2-(2-(4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenoxy)ethoxy)ethoxy)ethanol

There total 3 articles about 2-(2-(2-(4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenoxy)ethoxy)ethoxy)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.4%

: 187662-48-2
2-(2-(2-(4-iodophenoxy)ethoxy)ethoxy)ethan-1-ol

: 17573-94-3,752235-18-0
4-ethynyl-N,N-dimethylaniline

: 946052-62-6
2-(2-(2-(4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenoxy)ethoxy)ethoxy)ethanol

Guidance literature:: With sodium azide; trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; sodium L-ascorbate; In water; dimethyl sulfoxide; at 20 ℃; for 24h; Product distribution / selectivity;

Reference yield:

: 5197-62-6
2-[2-(chloroethoxy)ethoxy]ethanol

: 946052-62-6
2-(2-(2-(4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenoxy)ethoxy)ethoxy)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / K₂CO₃ / NaI / dimethylformamide / 17 h / 110 °C

2: 65 percent / sodium ascorbate; Na₂CO₃; NaN₃ / CuSO₄; L-proline / dimethylsulfoxide; H₂O / 24 h / 65 °C

With sodium azide; sodium carbonate; potassium carbonate; sodium L-ascorbate; copper(II) sulfate; L-proline; sodium iodide; In water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm070467l

Reference yield:

: 540-38-5
p-Iodophenol

: 946052-62-6
2-(2-(2-(4-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)phenoxy)ethoxy)ethoxy)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / K₂CO₃ / NaI / dimethylformamide / 17 h / 110 °C

2: 65 percent / sodium ascorbate; Na₂CO₃; NaN₃ / CuSO₄; L-proline / dimethylsulfoxide; H₂O / 24 h / 65 °C

With sodium azide; sodium carbonate; potassium carbonate; sodium L-ascorbate; copper(II) sulfate; L-proline; sodium iodide; In water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm070467l