(2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-1,2,3,4-octadecanetetraol

Base Information

Chemical Name:(2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-1,2,3,4-octadecanetetraol
CAS No.:129831-88-5
Molecular Formula:C₄₀H₅₈O₆S
Molecular Weight:666.963
Hs Code.:

Synonyms:(2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-1,2,3,4-octadecanetetraol

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Chemical Property of (2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-1,2,3,4-octadecanetetraol

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Technology Process of (2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-1,2,3,4-octadecanetetraol

There total 20 articles about (2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-1,2,3,4-octadecanetetraol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 129779-75-5,129831-87-4
(2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-5-octadecene-1,2,3,4-tetraol

: 129831-88-5
(2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-1,2,3,4-octadecanetetraol

Guidance literature:: With sodium acetate; toluene-4-sulfonic acid hydrazide; In ethanol; water; for 5h; Heating;

Reference yield:

: 20672-66-6,40246-26-2,84926-76-1,114179-79-2,115184-49-1
3,4,5-tri-O-benzyl-D-galactopyranose

: 129831-88-5
(2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-1,2,3,4-octadecanetetraol

Guidance literature:: Multi-step reaction with 4 steps

1: NaIO₄ / ethanol; H₂O / 16 h / -5 - 20 °C

2: 1.) nBuLi / 1.) hexane, THF, -10 deg C, 30 min, 2.) hexane, THF, RT, 16 h

3: H₂ / 10percent Pd/C / tetrahydrofuran / 16 h

4: pyridine / 1.5 h / 20 °C

With pyridine; sodium periodate; n-butyllithium; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm00012a018

Reference yield:

: 115563-43-4
(2S,3S,4R)-2,3,5-tribenzyloxy-4-hydroxypentanal

: 129831-88-5
(2R,3S,4R)-1,3,4-tri-O-benzyl-2-O-methansulfonyl-1,2,3,4-octadecanetetraol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) nBuLi / 1.) hexane, THF, -10 deg C, 30 min, 2.) hexane, THF, RT, 16 h

2: H₂ / 10percent Pd/C / tetrahydrofuran / 16 h

3: pyridine / 1.5 h / 20 °C

With pyridine; n-butyllithium; hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jm00012a018