2-(furfuryloxymethyl)benzyloxyacetic acid ethyl ester

Base Information

Chemical Name:2-(furfuryloxymethyl)benzyloxyacetic acid ethyl ester
CAS No.:251961-50-9
Molecular Formula:C₁₇H₂₀O₅
Molecular Weight:304.343
Hs Code.:

Synonyms:2-(furfuryloxymethyl)benzyloxyacetic acid ethyl ester

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Chemical Property of 2-(furfuryloxymethyl)benzyloxyacetic acid ethyl ester

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Technology Process of 2-(furfuryloxymethyl)benzyloxyacetic acid ethyl ester

There total 6 articles about 2-(furfuryloxymethyl)benzyloxyacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 251961-48-5
2-(furfuryloxymethyl)benzyl alcohol

: 105-36-2
ethyl bromoacetate

: 251961-50-9
2-(furfuryloxymethyl)benzyloxyacetic acid ethyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 2h; Heating;
DOI:10.1021/ol990168t

Reference yield:

: C₁₉H₂₈SiO₃

: 251961-50-9
2-(furfuryloxymethyl)benzyloxyacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.70 g / tetrabutylammonium fluoride / tetrahydrofuran / 2 h

2: 56 percent / sodium hydride / tetrahydrofuran / 2 h / Heating

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ol990168t

Reference yield:

: 81168-17-4
2-(tert-butyldimethylsiloxymethyl)benzyl alcohol

: 251961-50-9
2-(furfuryloxymethyl)benzyloxyacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / CH₂Cl₂ / 1.5 h / 0 °C

2: sodium hydride / tetrahydrofuran / 6 h

3: 1.70 g / tetrabutylammonium fluoride / tetrahydrofuran / 2 h

4: 56 percent / sodium hydride / tetrahydrofuran / 2 h / Heating

With tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol990168t