1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

Base Information

• Chemical Name: 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester
• CAS No.: 206976-38-7
• Molecular Formula: C₁₂H₁₂N₄O₄
• Molecular Weight: 276.252

Synonyms:1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

Chemical Property of 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

Chemical Property:

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Technology Process of 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

There total 2 articles about 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

4-azido-3-nitro-toluene (20615-75-2) → 6-methylbenzofuroxan (3524-05-8) + 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester (206976-38-7) + 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4,5-dicarboxylic acid 4-ethyl ester + 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4,5-dicarboxylic acid diethyl ester (206976-22-9)

Guidance literature:

With sodium 1,4-diethoxy-1,4-dioxobut-2-en-2-olate; In ethanol; at 50 ℃; for 22h; Further byproducts given;

DOI:10.1016/S0223-5234(98)80036-6

Reference yield: 32.0%

4-azido-3-nitro-toluene (20615-75-2) + diethyl oxalacetate sodium salt → 6-methylbenzofuroxan (3524-05-8) + 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester (206976-38-7) + 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4,5-dicarboxylic acid 4-ethyl ester + 1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4,5-dicarboxylic acid diethyl ester (206976-22-9)

Guidance literature:

In ethanol; at 50 ℃; for 22h; Further byproducts given;

DOI:10.1016/S0223-5234(98)80036-6

Reference yield: 95.0%

1-(4-Methyl-2-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester (206976-38-7) → 1-(2-Amino-4-methyl-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; Ambient temperature;

DOI:10.1016/S0223-5234(98)80036-6

upstream raw materials:

4-azido-3-nitro-toluene

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