N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-2,6-di-O-methanesulfonyl-D-glucitol

Base Information

Chemical Name:N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-2,6-di-O-methanesulfonyl-D-glucitol
CAS No.:176300-11-1
Molecular Formula:C₂₉H₃₅NO₈S₂
Molecular Weight:589.731
Hs Code.:

Synonyms:N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-2,6-di-O-methanesulfonyl-D-glucitol

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Chemical Property of N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-2,6-di-O-methanesulfonyl-D-glucitol

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Technology Process of N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-2,6-di-O-methanesulfonyl-D-glucitol

There total 7 articles about N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-2,6-di-O-methanesulfonyl-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124-63-0
methanesulfonyl chloride

: 157363-86-5
N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

: 176300-11-1
N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-2,6-di-O-methanesulfonyl-D-glucitol

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1016/S0968-0896(96)00266-0

Reference yield:

: 36199-02-7
3,4-di-O-benzyl-D-mannitol

: 176300-11-1
N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-2,6-di-O-methanesulfonyl-D-glucitol

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / imidazole / dimethylformamide / 2 h / 0 °C

2: NEt₃ / CH₂Cl₂ / 0.25 h / 0 °C

3: concd. aq. HCl / methanol / 2 h / 20 °C

4: 20percent aq. KOH / methanol / 3 h / 20 °C

5: 9 percent / aq. HClO₄ / 4 h / 20 °C

6: 100 percent / NEt₃ / CH₂Cl₂ / 0.17 h / 0 °C

With 1H-imidazole; hydrogenchloride; potassium hydroxide; perchloric acid; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(96)00266-0

Reference yield:

: 172147-86-3
Methanesulfonic acid (1R,2S,3S,4R)-2,3-bis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-4-methanesulfonyloxy-pentyl ester

: 176300-11-1
N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-2,6-di-O-methanesulfonyl-D-glucitol

Guidance literature:: Multi-step reaction with 4 steps

1: concd. aq. HCl / methanol / 2 h / 20 °C

2: 20percent aq. KOH / methanol / 3 h / 20 °C

3: 9 percent / aq. HClO₄ / 4 h / 20 °C

4: 100 percent / NEt₃ / CH₂Cl₂ / 0.17 h / 0 °C

With hydrogenchloride; potassium hydroxide; perchloric acid; triethylamine; In methanol; dichloromethane;
DOI:10.1016/S0968-0896(96)00266-0