Technology Process of C16H24ClNO7S
There total 4 articles about C16H24ClNO7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydrogencarbonate / water; acetonitrile / 2 h / 0 - 20 °C / Inert atmosphere
2.1: potassium hydrogencarbonate / acetonitrile / 72 h / 80 °C / Inert atmosphere
3.1: sodium iodide / acetone / 20 h / 20 °C / Inert atmosphere
3.2: polymer-supported triphenylphosphine / 1.67 h / 0 - 20 °C / Inert atmosphere
3.3: 4.17 h / 0 - 20 °C / Inert atmosphere
With
sodium hydrogencarbonate; potassium hydrogencarbonate; sodium iodide;
In
water; acetone; acetonitrile;
2.1: |Michael Addition;
DOI:10.1016/j.tet.2011.10.100
- Guidance literature:
-
C18H29NO8S;
With
sodium iodide;
In
acetone;
at 20 ℃;
for 20h;
Inert atmosphere;
In
dichloromethane;
at 0 - 20 ℃;
for 1.66667h;
Inert atmosphere;
With
thionyl chloride;
In
dichloromethane;
at 0 - 20 ℃;
for 4.16667h;
Inert atmosphere;
DOI:10.1016/j.tet.2011.10.100
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydrogencarbonate / acetonitrile / 72 h / 80 °C / Inert atmosphere
2.1: sodium iodide / acetone / 20 h / 20 °C / Inert atmosphere
2.2: polymer-supported triphenylphosphine / 1.67 h / 0 - 20 °C / Inert atmosphere
2.3: 4.17 h / 0 - 20 °C / Inert atmosphere
With
potassium hydrogencarbonate; sodium iodide;
In
acetone; acetonitrile;
1.1: |Michael Addition;
DOI:10.1016/j.tet.2011.10.100
