1-(2,6-diisopropylphenyl)-2-(3-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenoxy)phenyl)-1H-imidazole

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Chemical Name:1-(2,6-diisopropylphenyl)-2-(3-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenoxy)phenyl)-1H-imidazole
CAS No.:1395093-26-1
Molecular Formula:C₄₃H₄₈N₄O
Molecular Weight:636.88
Hs Code.:

Synonyms:1-(2,6-diisopropylphenyl)-2-(3-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenoxy)phenyl)-1H-imidazole

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Chemical Property of 1-(2,6-diisopropylphenyl)-2-(3-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenoxy)phenyl)-1H-imidazole

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Technology Process of 1-(2,6-diisopropylphenyl)-2-(3-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenoxy)phenyl)-1H-imidazole

There total 7 articles about 1-(2,6-diisopropylphenyl)-2-(3-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenoxy)phenyl)-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1404169-10-3
2-(3-bromophenyl)-1-(2,6-diisopropylphenyl)-1H-imidazole

: 1395093-25-0
3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenol

: 1395093-26-1
1-(2,6-diisopropylphenyl)-2-(3-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenoxy)phenyl)-1H-imidazole

Guidance literature:: With 2-Picolinic acid; copper(l) iodide; potassium phosphate monohydrate; In dimethyl sulfoxide; at 200 ℃; Inert atmosphere;

Reference yield:

: 100-84-5
1-methoxy-3-methyl-benzene

: 1395093-26-1
1-(2,6-diisopropylphenyl)-2-(3-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenoxy)phenyl)-1H-imidazole

Guidance literature:: Multi-step reaction with 6 steps

1.1: 4,4'-di-tert-butyl-2,2'-bipyridine / (1,5-cyclooctadiene)(methoxy)iridium(I) dimer / tetrahydrofuran / 80 °C / Sealed vessel

2.1: cesium fluoride; copper(II) nitrate trihydrate / water; methanol / 100 °C / Sealed vessel

3.1: trimethylaluminum / toluene / 2 h / 20 °C / Cooling; Inert atmosphere

3.2: 70 °C / Inert atmosphere

4.1: sodium hydrogencarbonate / isopropyl alcohol / 3 h / Reflux; Inert atmosphere

5.1: pyridine hydrochloride / 4 h / 190 °C / Inert atmosphere

6.1: copper(l) iodide; potassium phosphate monohydrate; 2-Picolinic acid / dimethyl sulfoxide / 200 °C / Inert atmosphere

With 2-Picolinic acid; copper(l) iodide; potassium phosphate monohydrate; copper(II) nitrate trihydrate; trimethylaluminum; pyridine hydrochloride; sodium hydrogencarbonate; cesium fluoride; 4,4'-di-tert-butyl-2,2'-bipyridine; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; isopropyl alcohol; toluene;

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1395093-26-1
1-(2,6-diisopropylphenyl)-2-(3-(3-(1-(2,6-diisopropylphenyl)-1H-imidazol-2-yl)-5-methylphenoxy)phenyl)-1H-imidazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: trimethylaluminum / toluene / 2 h / 20 °C / Cooling; Inert atmosphere

1.2: 70 °C / Inert atmosphere

2.1: sodium hydrogencarbonate / isopropyl alcohol / 3 h / Reflux; Inert atmosphere

3.1: pyridine hydrochloride / 4 h / 190 °C / Inert atmosphere

4.1: copper(l) iodide; potassium phosphate monohydrate; 2-Picolinic acid / dimethyl sulfoxide / 200 °C / Inert atmosphere

With 2-Picolinic acid; copper(l) iodide; potassium phosphate monohydrate; trimethylaluminum; pyridine hydrochloride; sodium hydrogencarbonate; In dimethyl sulfoxide; isopropyl alcohol; toluene;