((C(CH₃)3)2C₆H₃)4C₂₀H₆N₄ZnC₈H₂N₄C₁₀H₄N₂(C₆H₄(CH₂)10O₆C₆H₄)

Base Information

• Chemical Name: ((C(CH₃)3)2C₆H₃)4C₂₀H₆N₄ZnC₈H₂N₄C₁₀H₄N₂(C₆H₄(CH₂)10O₆C₆H₄)
• CAS No.: 1019647-90-5
• Molecular Formula: C₁₁₆H₁₂₄N₁₀O₆Zn
• Molecular Weight: 1819.71

Synonyms:((C(CH₃)3)2C₆H₃)4C₂₀H₆N₄ZnC₈H₂N₄C₁₀H₄N₂(C₆H₄(CH₂)10O₆C₆H₄)

Chemical Property of ((C(CH₃)3)2C₆H₃)4C₂₀H₆N₄ZnC₈H₂N₄C₁₀H₄N₂(C₆H₄(CH₂)10O₆C₆H₄)

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Technology Process of ((C(CH₃)3)2C₆H₃)4C₂₀H₆N₄ZnC₈H₂N₄C₁₀H₄N₂(C₆H₄(CH₂)10O₆C₆H₄)

There total 1 articles about ((C(CH₃)3)2C₆H₃)4C₂₀H₆N₄ZnC₈H₂N₄C₁₀H₄N₂(C₆H₄(CH₂)10O₆C₆H₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

((C(CH3)3)2C6H3)4C20H6N4H2C8H2N4C10H4N2(C6H4(CH2)10O6C6H4) + zinc diacetate (557-34-6) → ((C(CH3)3)2C6H3)4C20H6N4ZnC8H2N4C10H4N2(C6H4(CH2)10O6C6H4) (1019647-90-5)

Guidance literature:

With ethylene diamine tetraacetic acid tetrasodium salt; In methanol; dichloromethane; ligand in boiled CH2Cl2 treated with 5 equiv. of Zn salt in CH3OH, refluxed for 6 h, evapd., extd.(CH2Cl2, H2O), org. layer concd., treated withNa4EDTA, stirred for 24 h; org. layer extd.(CH2Cl2), washed (satd. Na2SO4, brine, H2O), evapd.;

DOI:10.1002/ejic.200700177

Reference yield: 99.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + ((C(CH3)3)2C6H3)4C20H6N4ZnC8H2N4C10H4N2(C6H4(CH2)10O6C6H4) (1019647-90-5) + N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2 (1147855-92-2) → 2Zn(2+)*2Cu(1+)*2C116H124N10O6(2-)*N2C12H6(N4C29H27O)2*2PF6(1-)=(ZnC116H124N10O6)2Cu2(N2C12H6(N4C29H27O)2)(PF6)2

Guidance literature:

In dichloromethane; acetonitrile; under Ar atm. to soln. Zn complex in CH2Cl2 soln. Cu complex in MeCN andstirred for 1 h in the absence of light at room temp., ligand in CH2Cl2 was added and stirred for 3 days in the absence of light; solvent was evapd.;

Reference yield: 97.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + ((C(CH3)3)2C6H3)4C20H6N4ZnC8H2N4C10H4N2(C6H4(CH2)10O6C6H4) (1019647-90-5) + 2,9-bis-(4-methoxy-phenyl)-1,10-phenanthroline (89333-97-1) → ((C(CH3)3)2C6H3)4C20H6N4ZnC8H2N4C10H4N2(C6H4(CH2)10O6C6H4)Cu((CH3OC6H4)2C12H6N2)(1+)*PF6(1-)=C142H144N12O8CuZnPF6 (1062321-77-0)

Guidance literature:

In dichloromethane; acetonitrile; (Ar), stoich., soln. of Cu complex in CH3CN added to degassed soln. of Zn complex in CH2Cl2, stirred for 30 min, treated with degassed soln. of dianisyl ligand in CH2Cl2, stirred for 2 h; extd.(CH2Cl2/H2O), org. layer dried (MgSO4), evapd.;

DOI:10.1002/ejic.200700177

upstream raw materials:

zinc diacetate

Downstream raw materials:

((C(CH₃)3)2C₆H₃)4C₂₀H₆N₄ZnC₈H₂N₄C₁₀H₄N₂(C₆H₄(CH₂)10O₆C₆H₄)Cu((CH₃OC₆H₄)2C₁₂H₆N₂)⁽¹⁺⁾*PF₆^(1-)=C₁₄₂H₁₄₄N₁₂O₈CuZnPF₆

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