[2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane

Base Information

Chemical Name:[2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane
CAS No.:535975-30-5
Molecular Formula:C₂₁H₂₄F₂S₂Si
Molecular Weight:406.636
Hs Code.:

Synonyms:[2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane

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Chemical Property of [2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane

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Technology Process of [2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane

There total 3 articles about [2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 5425-44-5
2-Phenyl-[1,3]dithiane

: 535975-23-6
dimethyl(phenyl)(3,3,3-trifluoropropan-1-en-2-yl)silane

: 535975-30-5
[2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 3h;
DOI:10.1021/jo034718j

Reference yield: 89.0%

: 53178-41-9
2-lithio-2-phenyl-1,3-dithiane

: 535975-23-6
dimethyl(phenyl)(3,3,3-trifluoropropan-1-en-2-yl)silane

: 535975-30-5
[2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane

Guidance literature:: In tetrahydrofuran; at -78 - 0 ℃; for 3h;
DOI:10.1016/S0040-4039(02)02652-7

Reference yield:

: 768-33-2
phenyldimethylsilyl chloride

: 535975-30-5
[2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Mg / tetrahydrofuran / 17 h / -10 - 20 °C

2: 89 percent / n-BuLi / tetrahydrofuran; hexane / 3 h / -78 - 0 °C

With n-butyllithium; magnesium; In tetrahydrofuran; hexane;
DOI:10.1021/jo034718j