Lithium, (2-phenyl-1,3-dithian-2-yl)-

Base Information

Chemical Name:Lithium, (2-phenyl-1,3-dithian-2-yl)-
CAS No.:53178-41-9
Molecular Formula:C10H11LiS2
Molecular Weight:202.27
Hs Code.:
DSSTox Substance ID:DTXSID20484146
Mol file:53178-41-9.mol

Synonyms:Lithium, (2-phenyl-1,3-dithian-2-yl)-;53178-41-9;SCHEMBL1758218;DTXSID20484146;GOXJKCHXKMYZIF-UHFFFAOYSA-N;2-lithio-2-phenyl-1,3-dithiane

Suppliers and Price of Lithium, (2-phenyl-1,3-dithian-2-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Lithium, (2-phenyl-1,3-dithian-2-yl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:202.04622113
Heavy Atom Count:13
Complexity:129

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:[Li+].C1CS[C-](SC1)C2=CC=CC=C2

Technology Process of Lithium, (2-phenyl-1,3-dithian-2-yl)-

There total 1 articles about Lithium, (2-phenyl-1,3-dithian-2-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5425-44-5
2-Phenyl-[1,3]dithiane

: 53178-41-9
2-lithio-2-phenyl-1,3-dithiane

Guidance literature:: With (biphenylyldiphenylmethyl)lithium; In tetrahydrofuran; at 25 ℃; Rate constant; also with (biphenylylbenzyl)lithium;
DOI:10.1021/jo00110a044

Reference yield: 89.0%

: 53178-41-9
2-lithio-2-phenyl-1,3-dithiane

: 535975-23-6
dimethyl(phenyl)(3,3,3-trifluoropropan-1-en-2-yl)silane

: 535975-30-5
[2,2-difluoro-1-(2-phenyl-1,3-dithian-2-ylmethyl)vinyl]dimethylphenylsilane

Guidance literature:: In tetrahydrofuran; at -78 - 0 ℃; for 3h;
DOI:10.1016/S0040-4039(02)02652-7

Reference yield: 86.7%

: 57560-51-7
tricarbonyl(η(6)-diphenyl ether)chromium

: 53178-41-9
2-lithio-2-phenyl-1,3-dithiane

: 116449-62-8
C₆H₅C(C₆H₅)S(CH₂)3SCr(CO)3

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; addn. of soln. of Cr-compd. in THF at -78°C to a soln. of the Li-compd., warm to 0°C in 15 min, cooling again to -78°C, addn. of a soln. of the acid in THF; extn., chromy., recrystn. from acetone;