2-(1-piperazinyl)ethyl 2-(4-isobutylphenyl)propionate dihydrochloride

Base Information

Chemical Name:2-(1-piperazinyl)ethyl 2-(4-isobutylphenyl)propionate dihydrochloride
CAS No.:144027-90-7
Molecular Formula:C₁₉H₃₀N₂O₂*2ClH
Molecular Weight:391.381
Hs Code.:

Synonyms:2-(1-piperazinyl)ethyl 2-(4-isobutylphenyl)propionate dihydrochloride

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Chemical Property of 2-(1-piperazinyl)ethyl 2-(4-isobutylphenyl)propionate dihydrochloride

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Technology Process of 2-(1-piperazinyl)ethyl 2-(4-isobutylphenyl)propionate dihydrochloride

There total 5 articles about 2-(1-piperazinyl)ethyl 2-(4-isobutylphenyl)propionate dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(4-Isobutyl-phenyl)-propionic acid 2-(4-benzyl-piperazin-1-yl)-ethyl ester

: 144027-90-7
2-(1-piperazinyl)ethyl 2-(4-isobutylphenyl)propionate dihydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; at 50 ℃; for 1.5h; under 2585.7 Torr;
DOI:10.1002/jps.2600810210

Reference yield:

: 103-76-4
1-(2-hydroxyethyl)piperazine

: 144027-90-7
2-(1-piperazinyl)ethyl 2-(4-isobutylphenyl)propionate dihydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / NaHCO₃ / dimethylformamide / Ambient temperature

2: 59 percent

3: 4.8 g / HCl(gas.), H₂ / 5percent Pd/C / ethanol / 1.5 h / 50 °C / 2585.7 Torr

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/jps.2600810210

Reference yield:

: 3221-20-3
1-benzyl-4-(2-hydroxyethyl)piperazine

: 144027-90-7
2-(1-piperazinyl)ethyl 2-(4-isobutylphenyl)propionate dihydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent

2: 4.8 g / HCl(gas.), H₂ / 5percent Pd/C / ethanol / 1.5 h / 50 °C / 2585.7 Torr

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1002/jps.2600810210