C₄₈H₄₈N₂O₁₀

Base Information

• Chemical Name: C₄₈H₄₈N₂O₁₀
• CAS No.: 1446748-45-3
• Molecular Formula: C₄₈H₄₈N₂O₁₀
• Molecular Weight: 812.917
• Mol file: 1446748-45-3.mol

Synonyms:C₄₈H₄₈N₂O₁₀

Chemical Property of C₄₈H₄₈N₂O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₈H₄₈N₂O₁₀

There total 9 articles about C₄₈H₄₈N₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C55H56N2O13S (1446748-44-2) → C48H48N2O10 (1446748-45-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol401566r

Reference yield:

C33H46N2O9Si (1446748-41-9) → C48H48N2O10 (1446748-45-3)

Guidance literature:

Multi-step reaction with 4 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3: pyridine / 1 h / 0 °C / Inert atmosphere

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;

DOI:10.1021/ol401566r

Reference yield:

C48H50N2O11 (1446748-43-1) → C48H48N2O10 (1446748-45-3)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 1 h / 0 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

With pyridine; sodium hydride; In N,N-dimethyl-formamide; mineral oil;

DOI:10.1021/ol401566r

upstream raw materials:

C₃₃H₄₆N₂O₉Si

4,4’-dimethoxytrityl trifluoromethanesulfonate

C₅₄H₆₄N₂O₁₁Si

C₄₈H₅₀N₂O₁₁

Downstream raw materials:

C₃₃H₃₄N₂O₉

C₄₂H₅₁N₄O₁₀P