C₂₂H₂₄O

Base Information

Chemical Name:C₂₂H₂₄O
CAS No.:908124-98-1
Molecular Formula:C₂₂H₂₄O
Molecular Weight:304.432
Hs Code.:

Synonyms:C₂₂H₂₄O

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Chemical Property of C₂₂H₂₄O

Chemical Property:

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Technology Process of C₂₂H₂₄O

There total 4 articles about C₂₂H₂₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 853955-93-8
2,4-dimethyl-2-phenylethynyl-pent-4-en-1-ol

: 100-39-0
benzyl bromide

: 908124-98-1
C₂₂H₂₄O

Guidance literature:: 2,4-dimethyl-2-phenylethynyl-pent-4-en-1-ol; With tetra-(n-butyl)ammonium iodide; potassium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

benzyl bromide; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ja063384n

Reference yield:

: 908125-52-0
2,4-dimethyl-2-phenylethynyl-pent-4-enoic acid ethyl ester

: 908124-98-1
C₂₂H₂₄O

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiAlH₄ / diethyl ether / 0 °C

2.1: KH; tetrabutylammonium iodide / tetrahydrofuran / 0.5 h / 0 °C

2.2: tetrahydrofuran / 1 h / 0 °C

With lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; potassium hydride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja063384n

Reference yield:

: 1483-82-5
phenylethynyl chloride

: 908124-98-1
C₂₂H₂₄O

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA; HMPA / tetrahydrofuran; petroleum ether / -78 - 0 °C

1.2: 72 percent / tetrahydrofuran; petroleum ether / -78 - 20 °C

2.1: LiAlH₄ / diethyl ether / 0 °C

3.1: KH; tetrabutylammonium iodide / tetrahydrofuran / 0.5 h / 0 °C

3.2: tetrahydrofuran / 1 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; potassium hydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; Petroleum ether;
DOI:10.1021/ja063384n