4-Chloro-4'-acetylstilbene

Base Information

Chemical Name:4-Chloro-4'-acetylstilbene
CAS No.:62827-82-1
Molecular Formula:C16H13ClO
Molecular Weight:256.732
Hs Code.:
NSC Number:166571
DSSTox Substance ID:DTXSID70422038
Nikkaji Number:J2.275.066F,J3.123.384D
Wikidata:Q82233809

Synonyms:NSC166571;62827-82-1;4-Chloro-4'-acetylstilbene;DTXSID70422038;4'-[(E)-4-Chlorostyryl]acetophenone;NSC-166571

Suppliers and Price of 4-Chloro-4'-acetylstilbene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-Chloro-4'-acetylstilbene

Chemical Property:

Vapor Pressure:6.86E-07mmHg at 25°C
Boiling Point:408.7°C at 760 mmHg
Flash Point:229.5°C
Density:1.187g/cm³
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:256.0654927
Heavy Atom Count:18
Complexity:294

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=CC=C(C=C1)C=CC2=CC=C(C=C2)Cl
Isomeric SMILES:CC(=O)C1=CC=C(C=C1)/C=C/C2=CC=C(C=C2)Cl

Technology Process of 4-Chloro-4'-acetylstilbene

There total 3 articles about 4-Chloro-4'-acetylstilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 99-91-2
para-chloroacetophenone

: 62827-82-1
C₁₆H₁₃ClO

Guidance literature:: With tetrabutylammomium bromide; sodium acetate; C₂₇H₂₁FN₄O₂Pd; at 140 ℃; for 6h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejic.202000530

Reference yield: 90.0%

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 99-90-1
para-bromoacetophenone

: 62827-82-1
C₁₆H₁₃ClO

Guidance literature:: With trans-[PdBr₂(1-(3-triethylammonium)propyl-4-mesityl-1,2,4-triazolin-5-ylidene)₂]Br₂; potassium hydroxide; In water; isopropyl alcohol; at 120 ℃; for 4h; Catalytic behavior;
DOI:10.1021/acs.organomet.7b00329

Reference yield: 83.0%

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 13329-40-3
4-Iodoacetophenone

: 787-69-9
4,4'-diacetylbiphenyl

: 62827-82-1
C₁₆H₁₃ClO

: C₁₆H₁₃ClO

Guidance literature:: With C₃₂H₂₅ClNO₂PPd; triethylamine; at 130 ℃; for 1.5h; Catalytic behavior; Sealed tube; Green chemistry;
DOI:10.1016/j.mcat.2019.110406