tetramethylruthenocene

Base Information

Chemical Name:tetramethylruthenocene
CAS No.:264910-31-8
Molecular Formula:C₁₄H₁₈Ru
Molecular Weight:287.367
Hs Code.:

Synonyms:tetramethylruthenocene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetramethylruthenocene

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Technology Process of tetramethylruthenocene

There total 1 articles about tetramethylruthenocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14898-67-0
ruthenium trichloride hydrate

: 4249-10-9
1,2,3,4-tetramethylcyclopenta-1,3-diene

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 1287-13-4
bis(η⁵-cyclopentadienyl)ruthenium

: 123283-74-9
(η(5)-C5Me4H)2Ru

: 264910-31-8
tetramethylruthenocene

Guidance literature:: With zinc; In ethanol; under N2; Ru salt stirred in degassed EtOH until complete dissolution had occurred (2-3 h); 1 equiv. of cyclopentadiene added followed by 2.7 equiv. of tetramethylcyclopentadiene; Zn dust added slowly; heated at reflux for 6 h; solvent and volatiles removed under vac.; extd. with hot hexanes; filtered through Celite; filtrate purified on Al2O3 column (hexanes); solventremoved by rotary evapn.; mixt. of (Me4Cp)CpRu : Cp2Ru : (Me4Cp)2Ru = 46.7% : 21.4% : 31.9 %; without sepn.;
DOI:10.1021/ic990690b