(η(5)-C5Me4H)2Ru

Base Information

Chemical Name:(η(5)-C5Me4H)2Ru
CAS No.:123283-74-9
Molecular Formula:C₁₈H₂₆Ru
Molecular Weight:343.474
Hs Code.:

Synonyms:(η(5)-C5Me4H)2Ru

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Chemical Property of (η(5)-C5Me4H)2Ru

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Technology Process of (η(5)-C5Me4H)2Ru

There total 1 articles about (η(5)-C5Me4H)2Ru which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14898-67-0
ruthenium trichloride hydrate

: 4249-10-9
1,2,3,4-tetramethylcyclopenta-1,3-diene

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 1287-13-4
bis(η⁵-cyclopentadienyl)ruthenium

: 123283-74-9
(η(5)-C5Me4H)2Ru

: 264910-31-8
tetramethylruthenocene

Guidance literature:: With zinc; In ethanol; under N2; Ru salt stirred in degassed EtOH until complete dissolution had occurred (2-3 h); 1 equiv. of cyclopentadiene added followed by 2.7 equiv. of tetramethylcyclopentadiene; Zn dust added slowly; heated at reflux for 6 h; solvent and volatiles removed under vac.; extd. with hot hexanes; filtered through Celite; filtrate purified on Al2O3 column (hexanes); solventremoved by rotary evapn.; mixt. of (Me4Cp)CpRu : Cp2Ru : (Me4Cp)2Ru = 46.7% : 21.4% : 31.9 %; without sepn.;
DOI:10.1021/ic990690b