{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid

Base Information

Chemical Name:{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid
CAS No.:1413285-59-2
Molecular Formula:C₁₉H₁₃Cl₃F₃NO₂S
Molecular Weight:482.738
Hs Code.:

Synonyms:{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid

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Chemical Property of {2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid

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Technology Process of {2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid

There total 6 articles about {2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1413285-58-1
{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester

: 1413285-59-2
{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 403-16-7
3-chloro-4-fluorobenzoic acid

: 1413285-59-2
{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 18 h / 20 °C

1.2: 1 h / 20 °C

2.1: Lawessons reagent / toluene / 1 h / Reflux

3.1: potassium carbonate / butanone / 1 h / Inert atmosphere; Reflux

3.2: 16 h / 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / -5 - 0 °C

5.1: caesium carbonate / N,N-dimethyl-formamide / 130 °C

6.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With Lawessons reagent; oxalyl dichloride; tetrabutyl ammonium fluoride; potassium carbonate; caesium carbonate; N,N-dimethyl-formamide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; butanone;

Reference yield:

: 1413285-57-0
3-(3,5-dichlorophenyl)-5-(3-chloro-4-fluorophenyl)-3-trifluoromethyl-3,4-dihydro-2H-pyrrole

: 1413285-59-2
{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 130 °C

2: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With caesium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;