{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester

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Chemical Name:{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester
CAS No.:1413285-58-1
Molecular Formula:C₂₃H₂₁Cl₃F₃NO₂S
Molecular Weight:538.845
Hs Code.:

Synonyms:{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester

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Chemical Property of {2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester

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Technology Process of {2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester

There total 5 articles about {2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20291-99-0
t-butyl mercaptoacetate

: 1413285-57-0
3-(3,5-dichlorophenyl)-5-(3-chloro-4-fluorophenyl)-3-trifluoromethyl-3,4-dihydro-2H-pyrrole

: 1413285-58-1
{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 130 ℃;

Reference yield:

: 403-16-7
3-chloro-4-fluorobenzoic acid

: 1413285-58-1
{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 18 h / 20 °C

1.2: 1 h / 20 °C

2.1: Lawessons reagent / toluene / 1 h / Reflux

3.1: potassium carbonate / butanone / 1 h / Inert atmosphere; Reflux

3.2: 16 h / 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / -5 - 0 °C

5.1: caesium carbonate / N,N-dimethyl-formamide / 130 °C

With Lawessons reagent; oxalyl dichloride; tetrabutyl ammonium fluoride; potassium carbonate; caesium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; butanone;

Reference yield:

: 1413285-55-8
3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzamide

: 1413285-58-1
{2-chloro-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]phenylsulfanyl}acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / butanone / 1 h / Inert atmosphere; Reflux

1.2: 16 h / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / -5 - 0 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 130 °C

With tetrabutyl ammonium fluoride; potassium carbonate; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; butanone;