3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzimidic acid methyl ester

Base Information

Chemical Name:3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzimidic acid methyl ester
CAS No.:1413285-56-9
Molecular Formula:C₁₂H₁₇ClFNSSi
Molecular Weight:289.877
Hs Code.:

Synonyms:3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzimidic acid methyl ester

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Chemical Property of 3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzimidic acid methyl ester

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Technology Process of 3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzimidic acid methyl ester

There total 3 articles about 3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzimidic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1413285-55-8
3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzamide

: 74-88-4
methyl iodide

: 1413285-56-9
3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzimidic acid methyl ester

Guidance literature:: 3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzamide; With potassium carbonate; In butanone; for 1h; Inert atmosphere; Reflux;

methyl iodide; In butanone; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 403-16-7
3-chloro-4-fluorobenzoic acid

: 1413285-56-9
3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzimidic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 18 h / 20 °C

1.2: 1 h / 20 °C

2.1: Lawessons reagent / toluene / 1 h / Reflux

3.1: potassium carbonate / butanone / 1 h / Inert atmosphere; Reflux

3.2: 16 h / 20 °C / Inert atmosphere

With Lawessons reagent; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; toluene; butanone;

Reference yield:

: 1413285-54-7
3-chloro-4-fluoro-N-trimethylsilanylmethylbenzamide

: 1413285-56-9
3-chloro-4-fluoro-N-trimethylsilanylmethylthiobenzimidic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: Lawessons reagent / toluene / 1 h / Reflux

2.1: potassium carbonate / butanone / 1 h / Inert atmosphere; Reflux

2.2: 16 h / 20 °C / Inert atmosphere

With Lawessons reagent; potassium carbonate; In toluene; butanone;