C₂₄H₁₉F₂IN₂O₇

Base Information

Chemical Name:C₂₄H₁₉F₂IN₂O₇
CAS No.:1613591-16-4
Molecular Formula:C₂₄H₁₉F₂IN₂O₇
Molecular Weight:612.325
Hs Code.:

C<sub>24</sub>H<sub>19</sub>F<sub>2</sub>IN<sub>2</sub>O<sub>7</sub>

Synonyms:C₂₄H₁₉F₂IN₂O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₁₉F₂IN₂O₇

Chemical Property:

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Technology Process of C₂₄H₁₉F₂IN₂O₇

There total 12 articles about C₂₄H₁₉F₂IN₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22224-41-5
1,3,5-tri-O-benzoyl-α-D-ribofuranoside

: 1613591-16-4
C₂₄H₁₉F₂IN₂O₇

Guidance literature:: Multi-step reaction with 16 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / acetonitrile / 12 h / Reflux

2.1: tetrahydrofuran / 1 h / -78 - 30 °C

2.2: 12 h / 20 °C

3.1: NOBSA / acetonitrile / 1.5 h / Reflux

3.2: 12 h / 60 - 70 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

5.1: methanol; sodium methylate / dichloromethane / 2.5 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

6.2: 12 h / 20 °C

7.1: water; 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran / 24 h / 20 °C

8.1: sodium periodate / tetrahydrofuran; methanol; water / 2 h / 20 °C

8.2: 0.5 h / 0 - 20 °C

9.1: dmap / dichloromethane / 0.67 h / 0 - 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 72 h / 70 - 80 °C

11.1: ammonium cerium (IV) nitrate / acetonitrile; water / 20 °C

12.1: boron trichloride / dichloromethane / 2 h / -70 °C

13.1: triphenylphosphine; pyridine; iodine / 12 h / 0 - 20 °C / Inert atmosphere

14.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; acetonitrile / 2 h / 60 - 70 °C

15.1: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 2 h / 0 - 20 °C

16.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

With pyridine; methanol; dmap; sodium periodate; N-iodo-succinimide; osmium(VIII) oxide; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; water; iodine; sodium methylate; boron trichloride; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); triethylamine; triphenylphosphine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 510765-51-2
2'-C-β-fluoromethyluridine

: 1613591-16-4
C₂₄H₁₉F₂IN₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; pyridine; iodine / 12 h / 0 - 20 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; acetonitrile / 2 h / 60 - 70 °C

3: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 2 h / 0 - 20 °C

4: dmap; triethylamine / dichloromethane / 12 h / 20 °C

With pyridine; dmap; N-iodo-succinimide; iodine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 1613591-13-1
5'-deoxy-5'-iodo-2'-C-(fluoromethyl)uridine

: 1613591-16-4
C₂₄H₁₉F₂IN₂O₇

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; acetonitrile / 2 h / 60 - 70 °C

2: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 2 h / 0 - 20 °C

3: dmap; triethylamine / dichloromethane / 12 h / 20 °C

With dmap; N-iodo-succinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;