N-(3-(4-bromo-2-nitrophenylamino)-5-(2-oxopyridin-1(2H)-yl)phenyl)-acetamide

Base Information

Chemical Name:N-(3-(4-bromo-2-nitrophenylamino)-5-(2-oxopyridin-1(2H)-yl)phenyl)-acetamide
CAS No.:1430728-55-4
Molecular Formula:C₁₉H₁₅BrN₄O₄
Molecular Weight:443.256
Hs Code.:

Synonyms:N-(3-(4-bromo-2-nitrophenylamino)-5-(2-oxopyridin-1(2H)-yl)phenyl)-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-(4-bromo-2-nitrophenylamino)-5-(2-oxopyridin-1(2H)-yl)phenyl)-acetamide

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Technology Process of N-(3-(4-bromo-2-nitrophenylamino)-5-(2-oxopyridin-1(2H)-yl)phenyl)-acetamide

There total 6 articles about N-(3-(4-bromo-2-nitrophenylamino)-5-(2-oxopyridin-1(2H)-yl)phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 364-73-8
4-Bromo-1-fluoro-2-nitrobenzene

: 1430728-54-3
N-(3-amino-5-(2-oxopyridin-1(2H)-yl)phenyl)acetamide

: 1430728-55-4
N-(3-(4-bromo-2-nitrophenylamino)-5-(2-oxopyridin-1(2H)-yl)phenyl)-acetamide

Guidance literature:: With potassium fluoride; In N,N-dimethyl-formamide; at 150 ℃; for 2h;

Reference yield:

: 18242-39-2
3,5-dinitrobromobenzene

: 1430728-55-4
N-(3-(4-bromo-2-nitrophenylamino)-5-(2-oxopyridin-1(2H)-yl)phenyl)-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid; iron / acetic acid / 0.5 h / 90 °C

2: 0.5 h / 0 - 20 °C

3: potassium carbonate; copper(l) iodide; trans-1,2-Diaminocyclohexane / toluene / 16 h / 100 °C

4: water; calcium chloride; iron / ethanol / 4 h / 100 °C

5: potassium fluoride / N,N-dimethyl-formamide / 2 h / 150 °C

With potassium fluoride; copper(l) iodide; trans-1,2-Diaminocyclohexane; water; iron; potassium carbonate; acetic acid; calcium chloride; In ethanol; acetic acid; N,N-dimethyl-formamide; toluene;

Reference yield:

: 99-65-0
meta-dinitrobenzene

: 1430728-55-4
N-(3-(4-bromo-2-nitrophenylamino)-5-(2-oxopyridin-1(2H)-yl)phenyl)-acetamide

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / 12.5 h / 0 - 20 °C

2: acetic acid; iron / acetic acid / 0.5 h / 90 °C

3: 0.5 h / 0 - 20 °C

4: potassium carbonate; copper(l) iodide; trans-1,2-Diaminocyclohexane / toluene / 16 h / 100 °C

5: water; calcium chloride; iron / ethanol / 4 h / 100 °C

6: potassium fluoride / N,N-dimethyl-formamide / 2 h / 150 °C

With potassium fluoride; copper(l) iodide; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; sulfuric acid; trans-1,2-Diaminocyclohexane; water; iron; potassium carbonate; acetic acid; calcium chloride; In ethanol; acetic acid; N,N-dimethyl-formamide; toluene;