2-hydroxy-3,5-diiodobenzoic acid ethyl ester

Base Information

• Chemical Name: 2-hydroxy-3,5-diiodobenzoic acid ethyl ester
• CAS No.: 528-15-4
• Molecular Formula: C₉H₈I₂O₃
• Molecular Weight: 417.97
• Mol file: 528-15-4.mol

Synonyms:2-hydroxy-3,5-diiodobenzoic acid ethyl ester

Chemical Property of 2-hydroxy-3,5-diiodobenzoic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-hydroxy-3,5-diiodobenzoic acid ethyl ester

There total 4 articles about 2-hydroxy-3,5-diiodobenzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-hydroxy-benzoic acid ethyl ester (118-61-6) → 2-hydroxy-3,5-diiodobenzoic acid ethyl ester (528-15-4)

Guidance literature:

With sodium hydrogencarbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate; In methanol; dichloromethane; for 7h; Ambient temperature;

DOI:10.1246/cl.1987.2109

Reference yield:

ethyl bromide (74-96-4) → 2-hydroxy-3,5-diiodobenzoic acid ethyl ester (528-15-4)

Guidance literature:

With ethanol;

Reference yield:

ethanol (64-17-5) + 3,5-diiodosalicylic acid (133-91-5) → 2-hydroxy-3,5-diiodobenzoic acid ethyl ester (528-15-4)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

ethanol

3,5-diiodosalicylic acid

2-hydroxy-benzoic acid ethyl ester

ethyl bromide

Downstream raw materials:

ethoxycarbonyl-6 diiodo-2,4 cyanatobenzene

ethyl 2-{[(4-chlorophenyl)sulfonyl]oxy}-3,5-diiodobenzoate

diiodo-2,8 phenylimino-2 benzoxazin-1,3 one-4