6-Chloro-3-(4-methoxy-3-methyl-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine

Base Information

Chemical Name:6-Chloro-3-(4-methoxy-3-methyl-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine
CAS No.:113628-65-2
Molecular Formula:C₁₇H₁₃ClN₄O
Molecular Weight:324.769
Hs Code.:

Synonyms:6-Chloro-3-(4-methoxy-3-methyl-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Chloro-3-(4-methoxy-3-methyl-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine

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Technology Process of 6-Chloro-3-(4-methoxy-3-methyl-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine

There total 3 articles about 6-Chloro-3-(4-methoxy-3-methyl-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 113628-51-6
N-(4-Chloro-phthalazin-1-yl)-N'-[1-(4-methoxy-3-methyl-phenyl)-meth-(E)-ylidene]-hydrazine

: 113628-65-2
6-Chloro-3-(4-methoxy-3-methyl-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine

Guidance literature:: With bromine; sodium acetate; In acetic acid; for 1h; Ambient temperature;
DOI:10.1021/jm00401a010

Reference yield:

: 51935-42-3,59275-72-8
1-chloro-4-hydrazinophthalazine

: 113628-65-2
6-Chloro-3-(4-methoxy-3-methyl-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 0.1N HCl / 0.17 h / 60 °C

2: 94 percent / Br₂, sodium acetate / acetic acid / 1 h / Ambient temperature

With hydrogenchloride; bromine; sodium acetate; In acetic acid;
DOI:10.1021/jm00401a010

Reference yield:

: 32723-67-4
3-methyl-4-anisaldehyde

: 113628-65-2
6-Chloro-3-(4-methoxy-3-methyl-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 0.1N HCl / 0.17 h / 60 °C

2: 94 percent / Br₂, sodium acetate / acetic acid / 1 h / Ambient temperature

With hydrogenchloride; bromine; sodium acetate; In acetic acid;
DOI:10.1021/jm00401a010