methyl 2,2-diphenyl-4-methyl-4-pentenoate

Base Information

Chemical Name:methyl 2,2-diphenyl-4-methyl-4-pentenoate
CAS No.:107556-97-8
Molecular Formula:C₁₉H₂₀O₂
Molecular Weight:280.367
Hs Code.:

Synonyms:methyl 2,2-diphenyl-4-methyl-4-pentenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,2-diphenyl-4-methyl-4-pentenoate

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Technology Process of methyl 2,2-diphenyl-4-methyl-4-pentenoate

There total 6 articles about methyl 2,2-diphenyl-4-methyl-4-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3469-00-9
methyl 2,2-diphenylacetate

: 563-47-3
3-Chloro-2-methylpropene

: 107556-97-8
methyl 2,2-diphenyl-4-methyl-4-pentenoate

Guidance literature:: methyl 2,2-diphenylacetate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

3-Chloro-2-methylpropene; In tetrahydrofuran; at -78 - 20 ℃; for 47h; Inert atmosphere;
DOI:10.1039/c0ob00701c

Reference yield: 75.0%

: 81112-28-9
methyl 2-methylprop-2-enyl carbonate

: 525-06-4
diphenyl ketene

: 107556-97-8
methyl 2,2-diphenyl-4-methyl-4-pentenoate

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;
DOI:10.1021/jo00385a009

Reference yield:

: 81112-28-9
methyl 2-methylprop-2-enyl carbonate

: 525-06-4
diphenyl ketene

: 77915-31-2
1,1’-(3-methyl-1,3-butadienylidene)bis-benzene

: 107556-97-8
methyl 2,2-diphenyl-4-methyl-4-pentenoate

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1039/c39860001539