(+/-)2,6-bis(1,1-dimethylethyl)-4-[(2S*-hydroxy-1R*-methylpropyl)-thio]phenol

Base Information

• Chemical Name: (+/-)2,6-bis(1,1-dimethylethyl)-4-[(2S*-hydroxy-1R*-methylpropyl)-thio]phenol
• CAS No.: 138752-87-1
• Molecular Formula: C₁₈H₃₀O₂S
• Molecular Weight: 310.501

Synonyms:(+/-)2,6-bis(1,1-dimethylethyl)-4-[(2S*-hydroxy-1R*-methylpropyl)-thio]phenol

Chemical Property of (+/-)2,6-bis(1,1-dimethylethyl)-4-[(2S*-hydroxy-1R*-methylpropyl)-thio]phenol

Chemical Property:

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Technology Process of (+/-)2,6-bis(1,1-dimethylethyl)-4-[(2S*-hydroxy-1R*-methylpropyl)-thio]phenol

There total 2 articles about (+/-)2,6-bis(1,1-dimethylethyl)-4-[(2S*-hydroxy-1R*-methylpropyl)-thio]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aqueous sodium chloride + 4-hydroxy-3,5-di-tert-butylthiophenol (950-59-4) + epoxy-2,3 butane (1758-32-3,1758-33-4,3266-23-7,6189-41-9,21490-63-1,63864-69-7,103110-88-9) → (+/-)2,6-bis(1,1-dimethylethyl)-4-[(2S*-hydroxy-1R*-methylpropyl)-thio]phenol (138752-87-1)

Guidance literature:

With hydrogenchloride; sodium methylate; magnesium sulfate; In methanol; hexane; ethyl acetate;

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + aqueous sodium chloride + 4-hydroxy-3,5-di-tert-butylthiophenol (950-59-4) + epoxy-2,3 butane (1758-32-3,1758-33-4,3266-23-7,6189-41-9,21490-63-1,63864-69-7,103110-88-9) → (+/-)2,6-bis(1,1-dimethylethyl)-4-[(2S*-hydroxy-1R*-methylpropyl)-thio]phenol (138752-87-1)

Guidance literature:

With sodium methylate; magnesium sulfate; In methanol; hexane; ethyl acetate;

Reference yield: 65.0%

(+/-)2,6-bis(1,1-dimethylethyl)-4-[(2S*-hydroxy-1R*-methylpropyl)-thio]phenol (138752-87-1) + bromoacetic acid tert-butyl ester (5292-43-3) → (+/-)tert-butyl[2S*-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-1R*-methylpropoxy]acetate

Guidance literature:

With acetic acid; In tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; hexane;

upstream raw materials:

4-hydroxy-3,5-di-tert-butylthiophenol

epoxy-2,3 butane

hydrogenchloride

Downstream raw materials:

(+/-)[2S*-[[3,5-bis(1,1-dimethyl-ethyl)-4-hydroxyphenyl]thio]-1R*-methylpropoxy]acetic acid

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