N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-4-methoxybenzylamine

Base Information

Chemical Name:N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-4-methoxybenzylamine
CAS No.:455885-65-1
Molecular Formula:C₂₆H₃₉NO
Molecular Weight:381.602
Hs Code.:

Synonyms:N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-4-methoxybenzylamine

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Chemical Property of N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-4-methoxybenzylamine

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Technology Process of N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-4-methoxybenzylamine

There total 3 articles about N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-4-methoxybenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: (4-Methoxy-benzyl)-[(2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trien-(E)-ylidene]-amine

: 1730-25-2
allylmagnesium bromide

: 455885-65-1
N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-4-methoxybenzylamine

Guidance literature:: In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(01)01179-0

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 455885-65-1
N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-4-methoxybenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: MgSO₄ / diethyl ether / 2 h / 0 °C

2: 912 mg / tetrahydrofuran; diethyl ether / 3.5 h / -40 - -25 °C

With magnesium sulfate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo0202233

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 455885-65-1
N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-4-methoxybenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: MgSO₄ / diethyl ether

2: 77 percent / tetrahydrofuran / 0 °C

With magnesium sulfate; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4039(01)01179-0