1-(4-methoxybenzyl)-6-(2,6,10-trimethyl-1E,5E,9-undecatrienyl)-5,6-dihydro-2(1H)-pyridone

Base Information

Chemical Name:1-(4-methoxybenzyl)-6-(2,6,10-trimethyl-1E,5E,9-undecatrienyl)-5,6-dihydro-2(1H)-pyridone
CAS No.:455885-67-3
Molecular Formula:C₂₇H₃₇NO₂
Molecular Weight:407.596
Hs Code.:

Synonyms:1-(4-methoxybenzyl)-6-(2,6,10-trimethyl-1E,5E,9-undecatrienyl)-5,6-dihydro-2(1H)-pyridone

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Chemical Property of 1-(4-methoxybenzyl)-6-(2,6,10-trimethyl-1E,5E,9-undecatrienyl)-5,6-dihydro-2(1H)-pyridone

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Technology Process of 1-(4-methoxybenzyl)-6-(2,6,10-trimethyl-1E,5E,9-undecatrienyl)-5,6-dihydro-2(1H)-pyridone

There total 6 articles about 1-(4-methoxybenzyl)-6-(2,6,10-trimethyl-1E,5E,9-undecatrienyl)-5,6-dihydro-2(1H)-pyridone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 455885-66-2
N-[4-methoxybenzyl]-N-[3,7,11-trimethyl-1-(2-propenyl)-2E,6E,10-dodecatrienyl]-2-propenamide

: 455885-67-3
1-(4-methoxybenzyl)-6-(2,6,10-trimethyl-1E,5E,9-undecatrienyl)-5,6-dihydro-2(1H)-pyridone

Guidance literature:: Grubbs catalyst first generation; In dichloromethane;
DOI:10.1016/S0040-4039(01)01179-0

Reference yield:

: 502-67-0
Farnesal

: 455885-67-3
1-(4-methoxybenzyl)-6-(2,6,10-trimethyl-1E,5E,9-undecatrienyl)-5,6-dihydro-2(1H)-pyridone

Guidance literature:: Multi-step reaction with 4 steps

1: MgSO₄ / diethyl ether / 2 h / 0 °C

2: 912 mg / tetrahydrofuran; diethyl ether / 3.5 h / -40 - -25 °C

3: 81 percent / triethylamine / tetrahydrofuran / 0 - 20 °C

4: 92 percent / Cl₂(PCy₃)2Ru=CHPh / CH₂Cl₂ / 1 h / Heating

With magnesium sulfate; triethylamine; Grubbs catalyst first generation; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo0202233

Reference yield:

: (4-Methoxy-benzyl)-[(2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trien-(E)-ylidene]-amine

: 455885-67-3
1-(4-methoxybenzyl)-6-(2,6,10-trimethyl-1E,5E,9-undecatrienyl)-5,6-dihydro-2(1H)-pyridone

Guidance literature:: Multi-step reaction with 3 steps

1: 912 mg / tetrahydrofuran; diethyl ether / 3.5 h / -40 - -25 °C

2: 81 percent / triethylamine / tetrahydrofuran / 0 - 20 °C

3: 92 percent / Cl₂(PCy₃)2Ru=CHPh / CH₂Cl₂ / 1 h / Heating

With triethylamine; Grubbs catalyst first generation; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo0202233