(E)-3--1-propanol

Base Information

Chemical Name:(E)-3--1-propanol
CAS No.:130487-29-5
Molecular Formula:C₁₆H₂₅NO₃
Molecular Weight:279.379
Hs Code.:

(E)-3-<p-(4-Dimethylaminooxy-3-methyl-2-butenyloxy)phenyl>-1-propanol

Synonyms:(E)-3--1-propanol

Suppliers and Price of (E)-3--1-propanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3--1-propanol

Chemical Property:

Purity/Quality:

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Technology Process of (E)-3--1-propanol

There total 6 articles about (E)-3--1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23795-02-0
3-(4-hydroxy-phenyl)-propionic acid ethyl ester

: 130487-29-5
(E)-3--1-propanol

Guidance literature:: Multi-step reaction with 5 steps

1: NaBr, K₂CO₃ / acetone / 24 h / Heating

2: 3.1 g / LiAlH₄ / diethyl ether / 1 h / 0 °C

3: 61percent Ca(OCl)2, aq. sat. sodium sulfate, dry ice / CH₂Cl₂ / 4 h

4: 2.72 g / ethanol; H₂O / 72 h / Ambient temperature

5: 1) sodium carbonate, peracetic acid / 1) dichloromethane, -60 deg C, 30 min, 2) 40-50 deg C, 1 h

With peracetic acid; lithium aluminium tetrahydride; calcium hypochlorite; Methamphetamin; sodium carbonate; potassium carbonate; sodium sulfate; sodium bromide; In diethyl ether; ethanol; dichloromethane; water; acetone;
DOI:10.1246/bcsj.63.1328

Reference yield:

: 501-97-3
4-hydroxyphenylpropionic acid

: 130487-29-5
(E)-3--1-propanol

Guidance literature:: Multi-step reaction with 6 steps

1: conc. sulfuric acid / benzene / 24 h / Heating

2: NaBr, K₂CO₃ / acetone / 24 h / Heating

3: 3.1 g / LiAlH₄ / diethyl ether / 1 h / 0 °C

4: 61percent Ca(OCl)2, aq. sat. sodium sulfate, dry ice / CH₂Cl₂ / 4 h

5: 2.72 g / ethanol; H₂O / 72 h / Ambient temperature

6: 1) sodium carbonate, peracetic acid / 1) dichloromethane, -60 deg C, 30 min, 2) 40-50 deg C, 1 h

With peracetic acid; lithium aluminium tetrahydride; calcium hypochlorite; sulfuric acid; Methamphetamin; sodium carbonate; potassium carbonate; sodium sulfate; sodium bromide; In diethyl ether; ethanol; dichloromethane; water; acetone; benzene;
DOI:10.1246/bcsj.63.1328

Reference yield:

: 61493-53-6
ethyl 3-[4-(3-methyl-but-2-enyloxy)phenyl]-propionate

: 130487-29-5
(E)-3--1-propanol

Guidance literature:: Multi-step reaction with 4 steps

1: 3.1 g / LiAlH₄ / diethyl ether / 1 h / 0 °C

2: 61percent Ca(OCl)2, aq. sat. sodium sulfate, dry ice / CH₂Cl₂ / 4 h

3: 2.72 g / ethanol; H₂O / 72 h / Ambient temperature

4: 1) sodium carbonate, peracetic acid / 1) dichloromethane, -60 deg C, 30 min, 2) 40-50 deg C, 1 h

With peracetic acid; lithium aluminium tetrahydride; calcium hypochlorite; Methamphetamin; sodium carbonate; sodium sulfate; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1246/bcsj.63.1328