(2S,4R)-1-O-t-butyldiphenylsilyl-5,5-bis(ethylthio)-1,2,4-pentanetriol

Base Information

Chemical Name:(2S,4R)-1-O-t-butyldiphenylsilyl-5,5-bis(ethylthio)-1,2,4-pentanetriol
CAS No.:116306-85-5
Molecular Formula:C₂₅H₃₈O₃S₂Si
Molecular Weight:478.792
Hs Code.:

Synonyms:(2S,4R)-1-O-t-butyldiphenylsilyl-5,5-bis(ethylthio)-1,2,4-pentanetriol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4R)-1-O-t-butyldiphenylsilyl-5,5-bis(ethylthio)-1,2,4-pentanetriol

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Technology Process of (2S,4R)-1-O-t-butyldiphenylsilyl-5,5-bis(ethylthio)-1,2,4-pentanetriol

There total 2 articles about (2S,4R)-1-O-t-butyldiphenylsilyl-5,5-bis(ethylthio)-1,2,4-pentanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 116306-84-4
(2S,4R)-5,5-bis(ethylthio)-1,2,4-pentanetriol

: 116306-85-5
(2S,4R)-1-O-t-butyldiphenylsilyl-5,5-bis(ethylthio)-1,2,4-pentanetriol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 25 ℃; for 0.5h;
DOI:10.1246/bcsj.60.4005

Reference yield:

: 3396-71-2
3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

: 116306-85-5
(2S,4R)-1-O-t-butyldiphenylsilyl-5,5-bis(ethylthio)-1,2,4-pentanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / boron trifluoride etherate / 2 h / Ambient temperature

2: 92 percent / imidazole / dimethylformamide / 0.5 h / 25 °C

With 1H-imidazole; boron trifluoride diethyl etherate; In N,N-dimethyl-formamide;
DOI:10.1246/bcsj.60.4005