(α)-2-(4-(5-(1,2-dithiolan-3-yl)pentanoyl)piperazin-1-yl)ethyl 4-acetoxy-3,5-dimethoxybenzoate

Base Information

Chemical Name:(α)-2-(4-(5-(1,2-dithiolan-3-yl)pentanoyl)piperazin-1-yl)ethyl 4-acetoxy-3,5-dimethoxybenzoate
CAS No.:1451180-80-5
Molecular Formula:C₂₅H₃₆N₂O₇S₂
Molecular Weight:540.702
Hs Code.:

Synonyms:(α)-2-(4-(5-(1,2-dithiolan-3-yl)pentanoyl)piperazin-1-yl)ethyl 4-acetoxy-3,5-dimethoxybenzoate

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Chemical Property of (α)-2-(4-(5-(1,2-dithiolan-3-yl)pentanoyl)piperazin-1-yl)ethyl 4-acetoxy-3,5-dimethoxybenzoate

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Technology Process of (α)-2-(4-(5-(1,2-dithiolan-3-yl)pentanoyl)piperazin-1-yl)ethyl 4-acetoxy-3,5-dimethoxybenzoate

There total 3 articles about (α)-2-(4-(5-(1,2-dithiolan-3-yl)pentanoyl)piperazin-1-yl)ethyl 4-acetoxy-3,5-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1451180-79-2
C₁₄H₂₆N₂O₂S₂

: 39657-47-1
O-acetylsyringic acid chloride

: 1451180-80-5
(α)-2-(4-(5-(1,2-dithiolan-3-yl)pentanoyl)piperazin-1-yl)ethyl 4-acetoxy-3,5-dimethoxybenzoate

Guidance literature:: C₁₄H₂₆N₂O₂S₂; With dmap; In dichloromethane; for 0.25h; Inert atmosphere;

O-acetylsyringic acid chloride; In dichloromethane; for 3h; Inert atmosphere; Cooling with ice;
DOI:10.5012/bkcs.2013.34.4.1025

Reference yield:

: 1200-22-2
(R)-1,2-dithiolane-3-pentanoic acid

: 1451180-80-5
(α)-2-(4-(5-(1,2-dithiolan-3-yl)pentanoyl)piperazin-1-yl)ethyl 4-acetoxy-3,5-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / Inert atmosphere

2.1: Inert atmosphere

3.1: dmap / dichloromethane / 0.25 h / Inert atmosphere

3.2: 3 h / Inert atmosphere; Cooling with ice

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.5012/bkcs.2013.34.4.1025

Reference yield:

: 1115175-97-7
2,5-dioxopyrrolidin-1-yl 5-(1,2-dithiolan-3-yl)pentanoate

: 1451180-80-5
(α)-2-(4-(5-(1,2-dithiolan-3-yl)pentanoyl)piperazin-1-yl)ethyl 4-acetoxy-3,5-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Inert atmosphere

2.1: dmap / dichloromethane / 0.25 h / Inert atmosphere

2.2: 3 h / Inert atmosphere; Cooling with ice

With dmap; In dichloromethane;
DOI:10.5012/bkcs.2013.34.4.1025